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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010537–000010557

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\ 03 04 02\2335.D Vial: 7 •Acq On 4 Mar 2002 3:11 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 7 Trisiloxane, 1,1,1,5,5,5-he... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

24.29 1.03 ug/L 538184 Phenanthrene-dl0 22.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamet... 384 C12H3604Si5 003555-47-3 38 2 SILICATE ANION TETRAMER 888 C24H72012Sil2 000000-00-0 38 3 3-Isopropoxy-1,1,1,7,7,7-hexamet... 576 C18H5207Si7 071579-69-6 38 4 VANILLYLPYRUVIC ACID 2TMS 354 C16H26O5S12 000000-00-0 37 Abundance Scan 2339 (24.291 min): 2335.D (-) m/z 73.10 100.00% 73

5000 147 221 281 24.00 24.20 24.40 24.60

m/z-> "7 117. 0+ TTT ‘ I MAa** 1911 21—4 ............................................. 50 100 150 200 250 300 350 400 450 500 550 m/z 147.10 38.97%

Abundance #322218: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trim... 73 147

281 5000 T T 24.00 24.20 24.40 24.60 m/z 221.10 23.98% 369 । 940 177 207 249. miz-> 0 474+ 117 rrfr ----- 338 | 50 100 150 200 250 300 350 400 450 500 550 I ' ‘ ' I • '' ‘ I • • ' ■ I •1 ■ u ■ ‘ ■ I ' ‘

Abundance #391009: SILICATE ANION TETRAMER 73

24.00 24.20 24*40 24.60 TT 5000 147 m/z 281.00 23.27%

221 28 281 | ■*I•।H। 401 01 ■ ■ ■ i ■ ■ • • i • ■ * * i • TIT T T m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #379639: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(tr... 73 T T T T 24.00 24.20 24.40 24.60 m/z 355.10 9.87%

5000 147 43 221 281 29- , 0 - :...... I.... 327 415....... 519 561 \ T ‘ T T /z—> 50 100 150 200 250 300 350 400 450 500 550 24.00 24.20 24.40 24.60

2335.D 5080302.M Mon Mar 18 08:31:26 2002 Page 9

NYC-WTC_000010550

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NYC-WTC_000010550Source: NYC Law Department, mirrored locally

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