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GCMS analysis report for sample AE02335, March 2002

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Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010537–000010557

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\030402\2335.D Vial: 7 ■ Acq On 4 Mar 2002 3:11 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 6 1,1,1,5,7,7,7-Heptamethyl-3— Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.41 1.38 ug/L 716845 Phenanthrene -dl0 22.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual l l,l,l,5,7,7,7-Heptarnethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 50 2 3-HYDROXYSTEARIC ACID 2TMS 444 C24H52O3Si2 000000-00-0 43 3 3-Trimethylsilyloxystearic acid,... 444 C24H5203Si2 000000-00-0 43 4 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 43 Abundance Scan 2132 (22.414 mln): 2335.D (-) m/z 73.10 100.00% 73

5000 147 221 11 T T T T 294 355 429 22.00 22.20 22.40 22.60 22.80 45 m/z-> 0- - 0 50 117.. 100 150 +191124941325.1401L 200 250 300 350 400 m/z 147.10 29.00%

Abundance #352530:1,1.1,5.7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy... 73

147 5000 267 i • 1 ■' i • ■ ■ • i 355 429 22.00 22.20 22.40 22.60 22.80 45 207 m/z 221.10 22.38%

0- ' 1 i Ti/z-> 0 50 100 150 200 250 300 350 400 Abundance #352740: 3-HYDROXYSTEARIC ACID 2TMS 73

T T T 22.00 22.20 22.40 22.60 22.80 5000 147 233 m/z 355.00 11.14%

43 429 313

0- 17 । । 44444 117 339 387 /z—> 0 50 100 150 200 250 300 350 400 Abundance #352741:3-Trimethylsilyloxystearic add, trimethylsilyl este 73 T T T T T 22.00 22.20 22.40 22.60 22.80 m/z 429.10 10.86%

5000 147 233

43 313 429 189

m/z—> 0 0 1444all 44 250..300.339. 50 100 387 . Tf 150 350 400 200 T T T T T 22.00 22.20 22.40 22.60 22.80

2335.D 5080302.M Mon Mar 18 08:31:25 2002 Page 8

NYC-WTC_000010549

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NYC-WTC_000010549Source: NYC Law Department, mirrored locally

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