NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\030402\2335.D Vial: 7
■ Acq On 4 Mar 2002 3:11 pm Operator: McLean
Sample 1/31 Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method ; C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
Peak Number 6 1,1,1,5,7,7,7-Heptamethyl-3— Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
22.41 1.38 ug/L 716845 Phenanthrene -dl0 22.53
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l l,l,l,5,7,7,7-Heptarnethyl-3,3-bi... 444 C13H40O5Si6 038147-00-1 50
2 3-HYDROXYSTEARIC ACID 2TMS 444 C24H52O3Si2 000000-00-0 43
3 3-Trimethylsilyloxystearic acid,... 444 C24H5203Si2 000000-00-0 43
4 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 43
Abundance Scan 2132 (22.414 mln): 2335.D (-) m/z 73.10 100.00%
73
5000
147
221 11 T T T T
294 355 429 22.00 22.20 22.40 22.60 22.80
45
m/z->
0- -
0 50
117..
100 150
+191124941325.1401L
200 250 300 350 400
m/z 147.10 29.00%
Abundance #352530:1,1.1,5.7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy...
73
147
5000 267 i • 1 ■' i • ■ ■ • i
355 429 22.00 22.20 22.40 22.60 22.80
45 207 m/z 221.10 22.38%
0- ' 1 i
Ti/z-> 0 50 100 150 200 250 300 350 400
Abundance #352740: 3-HYDROXYSTEARIC ACID 2TMS
73
T T T
22.00 22.20 22.40 22.60 22.80
5000 147 233 m/z 355.00 11.14%
43 429
313
0-
17 । ।
44444 117 339 387
/z—> 0 50 100 150 200 250 300 350 400
Abundance #352741:3-Trimethylsilyloxystearic add, trimethylsilyl este
73 T T T T T
22.00 22.20 22.40 22.60 22.80
m/z 429.10 10.86%
5000 147 233
43
313 429
189
m/z—>
0
0
1444all 44 250..300.339.
50 100
387 .
Tf
150
350 400 200
T T T T T
22.00 22.20 22.40 22.60 22.80
2335.D 5080302.M Mon Mar 18 08:31:25 2002 Page 8
NYC-WTC_000010549
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