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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010537–000010557

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\030402\2335.D Vial: 7 Acq On 4 Mar 2002 3:11 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 5 Benzeneacetic acid, .alpha.... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

20.31 1.75 ug/L 898144 Acenaphthene-dl0 18.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 40 2 Benzoic acid, 2,4-bis [ (trimethyl. . . 370 C16H3004Si3 010586-16-0 38 3 Benzoic acid, 2,6-bis[(trimethyl... 370 C16H30O4S13 003782-85-2 37 4 n-Nonadecanoic acid, pentamethyl... 428 C24H5202Si2 000000-00-0 35 Abundance Scan 1900 (20.309 min): 2335.D (-) m/z 73.10 100.00% 73

5000 147 355 221 11 111' i'1111 281 T T

m/z-> 45 0- — Abundance 50 117 191 11974+2494 100 150 200 250 300 350 400 450 zL 401

#361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 20.00 20.20 20.40 20.60 m/z 355.10 30.75%

73

5000 355 20.00 20.20 20.40 20.60 m/z 147.10 28.87% 147 47 105 [ 193 237 267295325 384 429457 0- stir pifiufg ri ri* TIr HTT n/z-> 50 100 150 200 250 300 350 400 450 Abundance #313243: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trim... 73 T TPT T 1 20.00 20.20 20.40 20.60 5000 m/z 221.10 23.51% 355 45

16 1 ,. 0- TIer 105123,163 193 223251 281 321 1 ........... m/z-> 50 100 150 200' ' 250 300 350 400 450 Abundance #313257: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trim... . ........... ... 73 355 20.00 20.20 20.40 20.60 m/z 281.10 16.33%

5000

147 267

m/z-> 0 44 1, ..

50 +1179207217 4313 100 150 200 250 300 ■ i' I* > > 11 1 1 ■1 i1 1 350 400 450 20.00 20.20 20'40 20.60

2335.D 5080302.M Mon Mar 18 08:31:24 2002 Page 7

NYC-WTC_000010548

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NYC-WTC_000010548Source: NYC Law Department, mirrored locally

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