NYC-WTC_000011415
Laboratory report documenting GCMS analysis of environmental sample AE03281 conducted on March 29, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS re-injection results, Sample 1639, Mar 2002
Machine-extracted title · confidence 100%Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
NYC-WTC_000012129–000012144Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
. Data File : C:\MSDCHEM\1\DATA\031902\1640.D Vial: 25 Acq On : 20 Mar 2002 10:32 am Operator: McLean Sample : RE-INJ 3/1 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 4 Benzoic acid, 2,6-bis[(trim... Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
20.28 0.96 ug/L 394940 Acenaphthene-dlO 18.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 2,6-bis[(trimethyl... 370 C16H30O4Si3 003782-85-2 37 2 n-Nonadecanoic acid, pentamethyl... 428 C24H5202Si2 000000-00-0 35 3 2-TRIMETHYLSILYLAMINO-1-TRIMETHY. . . 457 C20H43NO3Si4 068595-65-3 35 4 Benzoic acid, 2,5-bis(trimethyls... 370 C16H30O4Si3 003618-20-0 27 Abundance Scan 1897 (20.282 min): 1640.D (-) m/z 73.10 100.00% 73
5000 147 355 221 281 401 20.00 20.20 20.40 20.60 45 117 >7 , 191, , 251, [ 327 m/z 355.10 35.02% 0- - 1 ‘ 1 1 *Pe4 ■ ■ I 1 ' ■ ■ i ■ m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #313257: Benzoic add, 2,6-bis[(trimethylsiiyl)oxy]-, trim... 73 355
5000 20.00 20.20 20.40 20.60 267 m/z 147.10 31.36% 147 44 . . 119 I 179207 237 | , 313 0- 1 ‘'‘I r4 • <-> i 1 tin thpiyeni TI 42/22817 m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #346318: n-Nonadecanoic acid, pentamethyldisilyl ester 43 73 355 --- 20.00 20.20 20.40 20.60 147 m/z 221.10 26.18% 5000 413 203
miz—> 0 50 Alike 100 150 ll i 245 ' 295 325, । r. j . . .1 । > . >PITp . ii | Ppri ri | 1" 200 300 350 400 450 500 250 Abundance #357157:2-TRlMETHYLSILYLAMINO-1-TRIMETHYLSILYLOXY-1-(3',4. \.... 73 J “ ’11 20.00 20.20 20.40 20.60 m/z 281.10 16.74% 355
5000 102
45 486 , 147 179 207 251 281 ;325 , 381408 442 0 TH -mtf.PRTTmTr /z—> 50 100 150 200 250 300 350 400 450 500 20.00 20.20 20.40 20*60
1640.D 5080302.M Thu Mar 21 06:31:30 2002 Page 6
NYC-WTC_000012139
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NYC-WTC_000012139Source: NYC Law Department, mirrored locally
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