GCMS analysis report, sample AE02336, March 22, 2002

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*. Data File C:\MSDCHEM\1\DATA\030402\2336.D Vial: 8 Acq On 4 Mar 2002 4:00 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C: \DATABASE\WILEY7N. L

Peak Number 11 SILICONE POLYMER Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

32.82 0.46 ug/L 159515 Perylene-d12 34.21

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 SILICONE POLYMER 458 C14H4205Si6 000000-00-0 64 2 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72O12S112 018919-94-3 50 3 SILICATE ANION TETRAMER 888 C24H72O12Sil2 000000-00-0 45 4 2-METHYLPROPANTRIOL-l, 1,3-D3, TR... 325 C13H31D3O3Si3 000000-00-0 42 Abundance Scan 3279 (32.817 min): 2336.D (-) m/z 73.10 100.00% 73

5000 147 221

281 355 32.40 32.60 32.80 33.00 33.20 , 1 429 0- .*..... U, H , 1k k m/z 147.10 46.82% miz-> 50 100 150 200 250 300 350 400 Abundance #392084: SILICONE POLYMER 73

5000 147 111. A., 32.40 32.60 32.80 33.00 33.20 m/z 221.10 45.24% 221 109 43 182 | 249 281 O' - 44 —1l 1 * * •’ I I.4PTfTe m/z-> 50 100 150 200 250 300 350 400 Abundance#391010: TETRACOSAMETHYLCYCLODODECASILOXANE $$ Cyclod ) 73 355 T T T T T 32.40 32.60 32.80 33.00 33.20 147 221 281 m/z 281.00 23.53% 5000

415 3251 0- 45 s... 1 1%. 191 > ' 11 1 249 । (14" -'l — 1 385, | . mtz~> 50 100 150 200 250 300 350 400 Abundance 73 #391009: SILICATE ANION TETRAMER -A 32.40 32.60 32.80 33.00 33.20 m/z 207.00 18.70%

5000

m/z—> 0 28 l. . 50 100 147

221

-- 281 ............ 401 150 200 250 300 350 400 . i i U r T T 32.40 32.60 32.80 33.00 33.20

2336.D 5080302.M Mon Mar 18 08:31:54 2002 Page 13

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