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GCMS analysis results for sample AE03804, March 22, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.

NYC-WTC_000037948–000037963

Folder label: “GCMS X 2/20/02 A 3/20/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3804.D Vial: 14 Acq On : 19 Mar 2002 10:18 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Iron, monocarbonyl-(1,3-but... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

27.52 0.43 ug/L 191765 Chrysene-dl2 30.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Iron, monocarbonyl-(1,3-butadien... 438 C21H22FeN2O5 109007-87-6 58 2 BISTRIMETHYLSILYL N-ACETYL EICOS... 511 C28H57NO3Si2 000000-00-0 53 3 lH-Purin-6-amine, [(2-fluorophen... 243 C12H10FN5 074421-44-6 43 4 TETRACOSAMETHYLCYCLODODECASILOXA. . . 888 C24H72012Sil2 018919-94-3 43 Abundance Scan 2695 (27.520 min): 3804.D (-) m/z 73.05 100.00% 73

5000 147 221 281 355 429 —A 27.20 27.40 27.60 27.80 0 TH 1 “"I TITT ‘Il —pmppm m/z 147.10 45.82% m/z-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #350342: Iron, monocarbonyl-(1 ,3-butadiene-1 ,4-dicarbonic ... 73

147 221 — i -A------ r 5000 355 27.20 27.40 27.60 27.80 281 429 m/z. 221710 36711% 26 503

m/z—> 0 0 ulu nr Terr Trtttnm t i I 1 50 100 150 200 250 300 350 400 450 500 550 600 650 700 577 652

Abundance#370710: BISTRIMETHYLSILYL N-ACETYL EICOSASPHINGA-4,11-Dlt: 73

। < । । ‘ • V। < i <| < • > i | । । TT 27.20 27.40 27.60 27.80 m/z 355.1018.11% 5000 174 129 221 337 , 281 429 0V miz-> 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 Abundance #177443: 1H-Purin-6-amine, [(2-fluoropheny)methyl]- (CAS) TTT—rur T^1-? T 73 27.20 27.40 27.60 27.80 m/z 281.00 16.61% 28 147 221 5000 355 281 429 503

m/z—> 0 lkqlllllussss 0 50 100 150 200 250 300 350 400 450 500 550 600 650 700 563607 653 703 TTrrorrprr T-rrT-r-p-rT-r-r 27.20 27.40 27.60 27.80

- " 2003 2 M Page 10 Thu Mar 21 11:48:12 2002 NYC-WT C_000037962

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NYC-WTC_000037962Source: NYC Law Department, mirrored locally

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