GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Heneicosane (CAS) $$ n-Hene... Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

22.63 2.69 ug/L 413127 Phenanthrene-dlO 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 74 2 Nonadecane 268 C19H40 000629-92-5 72 3 Pentadecane 212 C15H32 000629-62-9 68 4 Octacosane 394 C28H58 000630-02-4 68 Abundance . Scan 3328 (22.633 min): 7115.D (-) m/z 57.10 100.00% 57 105

iililB 85

Tl/z-> Abundance 0 J 183 J ' I'''' I'''' I 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #245747: Heneicosane (CAS) $$ n-Heneicosane 246 I ' I' • ’ • I • " ' I 22.40 22.60 22.80 23.00 m/z 105.10 90.48%

s'?

5000 85 22.40 22.60 22.80 23.00 m/z 71.10 58.06% 4 ,1 239 296 0 ...... ' I' I'''' I'' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #211482; Nonadecane 57

22.40 22.60 22.80 23.00 5000 m/z 43.10 42.69% 4 85

268 VrTY’~rrTYTTTrpVrrjTTTrrp-i5njTTT-rpT^^ rn/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #134012: Pentadecane 5i7 22.40 22.60 22.80 23.00 m/z 85.15 40.90%

5000 85 4

212 0 ...... m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 22.40 22.60 22.80 23.00

7115.D 5080402BB.M Mon Apr 15 18:16:23 2002 Page 4

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