GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Cyclotetradecane Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

23.59 28.38 ug/L 4354900 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetradecane 196 C14H28 000295-17-0 93 2 9-Octadecene, (E)- 252 C18H36 007206-25-9 91 3 1-Hexadecene (CAS) $$ Cetene $$ ... 224 C16H32 000629-73-2 91 4 1-Pentadecanol_____________________________ 228 C15H32O 000629-76-5 91 Abundance Scan 3490 (23.585 min): 7115.D (-) m/z 55.10 10^70^% 55

69 83

97 I 4

23.20 23.40 23.60 23.80 24.00 OVr m/z 57.10 85.90% Tl/Z-> 20 40 60I 80 100 120 140 160 180 200 220 240 Abundance #110366: Cyclotetradecane 56 83 41 69

97 5000 111 196 23.20 23.40 23.60 23.80 24.00 m/z 83.10 78.79% 125

m/z-> 0 20 f 40 60 80 tex, 100 120 140 .160 180 200 220 240 Abundance #190572: 9-Octadecene, (El- 55

4’ 69 83 V 23 20 23.40 23.60 23.80 24.00 97 m/z 69.10 67779% TiTiTi!

111 2 125 I j' .‘'.y ^168182196 224 0 -p-rTrYTr-rT*rTT-r-rT-p-rT-rYT-i-rTt-p-rT-i-p-^ ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #152003:1-Hexadecene (CAS) S$ Cetene $$ 1-Cetene S$ n-Hex... 5^ 69 83 23'26 23.46 2^60 23.80 24.00 4 97 m/z 43.20 61.54%

5000 111

2’i 125

71/Z-> 0 j20X40i 60 80 I100 120 140 160 180 200 220 240 23.20 23.40 23.60 23.80 24.00

7115.D 5080402BB.M Mon Apr 15 18:16:24 2002 Page 5

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