GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Cyclohexane, methyl- (CAS) ... Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

25.15 2.47 ug/L 319050 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, methyl- (CAS) $$ Me... 98 C7H14 000108-87-2 38 2 1-Tetracosanol $$ n-Tetracosanol... 354 C24H50O 000506-51-4 38 3 1-Hexacosanol 382 C26H54O 000506-52-5 35 4 1-Octadecene 252 C18H36 000112-88-9 35 <\bundance Scan 3756 (25.148 min): 7110.D (-) “m/z 83.10 100.00% 83 57

5000

...Ui 111 "T , , 33153 179 24.80 25.00 25.20 25.40 0^ m/z 57.10 83.34% m/z-> 50 100 150 200 250 300 350 Abundance #7471: Cyclohexane, methyl- (CAS) S$ Methylcyclohexane $$ ... 56 83

5000 24.80 25.00 25.20 25.40 27 m/z 55.10 78.26%

0 ■n/z-> 100 150 200 250 300 350 Abundance #302105: 1-Tetracosanol SS n-Tetracosanol $$ Lignoceric al... 4i3

24.80 25.00 25.20 25.40 5000 83 m/z 43.10 72.91%

m/z-> Abundance 0 18 i 50 4(3 111

100 140 168 196 150 200 238 266 250 #321734; 1-Hexacosanol 308 336 300 350 'H' 'V 24.80 25.00 25.20 25.40 m/z 61.05 65.73%

5000 83

18

m/z-> 0 itU 50 111 ,1,1 100 150 168 196,224 252 278 308 336 364 200 250 300 350 IT 24.80 25.00 25.20 25.40 ■p

7110.D 5080402BB.M Mon Apr 15 17:09:16 2002 Page 9

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