GCMS sample AE07110 results, April 25, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 7 Cyclohexane, methyl- (CAS) ... Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

25.15 2.47 ug/L 319050 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclohexane, methyl- (CAS) $$ Me... 98 C7H14 000108-87-2 38 2 1-Tetracosanol $$ n-Tetracosanol... 354 C24H50O 000506-51-4 38 3 1-Hexacosanol 382 C26H540 000506-52-5 35 4 1-Octadecene 252 C18H36 000112-88-9 35 Abundance Scan 3756 (25.148 min): 7110.D (-) m/z 83.10 100.00%

L 83 57

5000

111 133153 179 24.80 25.00 25.20 25.40 1 - lL m/ z 57.10 83.34%

A 01 • ■ i • ■ • i ' miz-> 50 100 150 200 250 300 350 Abundance #7471: Cyclohexane, methyl- (CAS) $$ Methylcyclohexane S$... 55 83 Mw 5000 24*80 25.00 25.20 25*40 27 m/z 55.10 78.26%

m/z-> 0 Abundance 4444. 50 100 150 200 250 300 350 #302105: 1-Tetracosanol $5 n-Tetracosanol $$ Lignoceric al... M„Naw 43 ’1/6/0/2/-dr/-*121111117113 24.80 25.00 25.20 25.40 5000 83 m/z 43.10 72.91%

18

0- T*r“r Mil 111 ,1140 168 196 238 266 -r-r-]308 —i—r 336 ■ i • AWA Tl/z-> 50 100 ‘ 150 ’200 250' 300 350 Abundance #321734: 1-Hexacosanol 43 ‘ i ■ ■ ■ ‘ i1 ■ ‘ ■ i ‘ ■ i • • ■ ■ i • 24.80 25.00 25.20 25.40 m/z 61.05 65.73%

5000 83

m/z—> 0 18

l 50 A 111 1 4 .50 100 139— 168— 224 252 278 308 336 364 196— 150 200 250 300 350 ........................................... 24.80 25*66 25*20 25.40 ' *

7110.D 5080402BBC.M Tue Apr 23 15:52:15 2002 Page 9

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