GCMS sample AE07110 results, April 25, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 8 Benzenetriamine, ar,ar,ar-t... Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

25.30 1.19 ug/L 152982 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzenetriamine, ar,ar,ar-trinitro- 258 C6H6N606 067539-61-1 43 2 Benzoic acid, 4,4‘-oxybis- 258 C14H10O5 002215-89-6 43 3 9-Borabicyclo[3.3.1]nonane, 9,9'... 258 C16H28B2O 074744-62-0 43 4 2,3-diazatriptycene 258 C18H14N2 000000-00-0 38 Abundance Scan 3782 (25.301 min): 7110.D (-) m/z 258.20 100.00% 218

5000 43 65 81

95 121 135 11 155 175189 215 | a J ‘ ‘ ‘ ‘ I T 25.00 25.20 25.40 25.60 1

m/z-> O—PPT 20 40 T • i r J । » r। । |T» » I । « » » « । Ti ri । i r j t । j j j t । i i i i । i i » j“| i r 60 80 100 120 140 160 180 200 220 240 260 m/z 121.10 37.77%

Abundance #196672: Benzenetriamine, ar,ar,ar-trinitro- 268

5000 228 anisdd 11 25.00 25.20 25.40 25.60 67 m/z 81.10 32.66% 30 52 91 119

m/z-> 0 16.4 1164147365122. 211 242 T 1’188 20 40 60 80 100 120 140 160 180 200 220 240 260 fl AayyikwAuusy Abundance #197309: Benzoic acid, 4,4‘-oxybis- 268

I * * “ ! T 1‘ ' i 25.00 25.20 25.40 25.60 5000 241 m/z 71.10 30.08%

45 65

rn/z-> Abundance OSTTT 20 J 4 mm 92 115 141

40 60 80 100 120 140 160 180 200 220 240 260 #197955:9-Borabicyc!o[3.3.1]nonane, 9,9-oxybis- 218 168, MwM W.A I • ’ * ‘ I T T 1 25.00 25.20 25.40 25.60 m/z 43.10 29.49%

5000

0 ‘t1r 27 J 41 no

u. 1 7 189 7 120

T4.444.+.44.+*4203.1,+243.1 MWM WW. m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 25.00 25.20 25.40 25.60

7110.D 5080402BBC.M Tue Apr 23 15:52:16 2002 Page 10

NYC-WTC_000049049