Laboratory blank analysis results, sample AE10186, May 2002

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Library Search Compound Report

. Data File C:\MSDCHEM\l\DATA\050202\LBA0502.D Vial: 18 Acq On 2 May 2002 3:53 pm Operator: Bohlk / Inst 213 Sample LB 4/30/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library . : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 1,2-Benzenedicarboxylic aci... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

24.06 0.08 ug/L 157562 Phenanthrene d-10 21.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di... 530 C34H58O4 000119-06-2 50 2 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 47 3 Octacosane 394 C28H58 000630-02-4 38 4 Octadecane 254 C18H38 000593-45-3 38 Abundance Scan 1432 (24.065 min): LBA0502.D (-) m/z 57.05 100.00% 57 149 85

113 SEE

I I 207 329 377 T 23.80 24.00 24.20 24.40 0- ,)l.|ii|lil|il.i,!|iii.,i,l.... I ,.,i_____ m/z 149.10 95.12% •n/z-> 0 50 100 150 200 250 300 350 400 450 Abundance #373994:1,2-Benzenedicarboxylic acid, ditridecyl ester $$... 149

57 A SEB 23.80 24.00 24.20 24.40 85 m/z 71.15 93.71% 28 I .113

m/z-> 0- 0 Ai 50 100 ' 150 183 200 250 ' 300 349 350 ' 400 446 450 Abundance #275691: Tricosane (CAS) $S n-Tricosane 57

23.80 24.00 24.20 24.40 5000 85.10 73.51% 85

,253 281 324^ ....................... 0- m/z-> 0 50 100 150 200 250 300 350 400 4^ Abundance #329265: Octacosane 43 23.80 24.00 24.20 24.40 m/z 113.20 51.28% 71 5000

Tl/Z-> 0 - 0 50 99 J II r, 100 f 150 155 183 211 239 267 200 309 . i p-i ( i-j 1 r 250 300 351 ' I ' ' ' ' I ' ' ' ' I ' 350 400 450 4Uj 23.80 24.00 24.20 24.40

LBA0502.D 050102 .M Mon May 06 14:19:57 2002 Page 7

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