GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration.Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Benzenetriamine, ar,ar,ar-t... Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

25.30 1.19 ug/L 152982 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzenetriamine, ar,ar,ar-trinitro- 258 C6H6N6O6 067539-61-1 43 2 Benzoic acid, 4,4'-oxybis- 258 C14H10O5 002215-89-6 43 3 9-Borabicyclo[3.3.1]nonane, 9,9'... 258 C16H28B2O 074744-62-0 43 4 2,3-diazatriptycene 258 C18H14N2 000000-00-0 38 Abundance Scan 3782 (25.301 min): 7110.D (-) m/z 258.20 100.00% 258 ' 1 5000 121 43 81 135

'n/z-> Abundance 0 20 ulu 40 60 80 I5 215

100 120 140 160 180 200 220 240 260 #196672: Benzenetriamine, ar,ar,ar-trinitro- I ' ' ' ' I 25.00 25.20 25.40 25.60 m/z 121.10 37.77%

258

5000 228 iiilMA 25.00 25.20 25.40 2^60 67 m/z 81.10 32.66% !0 30 52 ®i' 242 0 ■n/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #197309: Benzoic acid, 4.4’-oxybis- 258

25.00 25.20 25.40 25.60 5000 241 m/z 71.10 30.08%

45 i. , 92 115 141 168 0 ' I'''' I' 'Sa m/z-> 20 40I 60 80 100 120 140 160 180 200 220 240 260 Abundance #197955: 9-Borabicyclo[3.3.1]nonane, 9,9'-oxybis- 258 25.00 25.20 25.40 25.60 m/z 43.10 29.49%

lililil 120 I [ 147 V I J L J - J i 162 189 217 27 oc^ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 25.00 25.20 25.40 25.60

7110.D 5080402BB.M Mon Apr 15 17:09:17 2002 Page 10

NYC-WTC_000061045