GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohllc Sample : SAMPLE 7110 3/27/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title Quantitation For Method 508gcscan Library C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 9 Tridecane, 7-hexyl- $$ 7-He... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

26.25 6.46 ug/L 775626 Chrysene-dl2 3 0.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane, 7-hexyl- $$ 7-Hexyltr... 268 C19H40 007225-66-3 90 2 Hexadecane 226 C16H34 000544-76-3 90 3 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 90 4 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 _______ 054833-48-6 89 Abundance Scan 3943 (26.247 min): 7110.D (-) m/z 57.10 100.00% 7

5000 85

4 I 26.00 26.20 26.40 26.60 TyrrrjL pJ- J, J T J J.f* ■ 169 , 196 215________ 296 m/z 71710 59.23% 0 |T.. q,tt, I n., f,.I, r,. p 1, 11,,.-I I,,,, I.,,. I,,,, I,., 11, m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #211476: Tridecane, 7-hexyl- SS 7-Hexyltridecane 57

29 5000 85 26.00 26.20 26.40 26.60 182 m/z 43.10 42.74%

0 211 238 266 TTJTTTTp-rTTYTT-TT-pT-rTJ-r-TTTy^ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #154905: Hexadecane 57

26.00 26.20 26.40 26.60 5000 m/z 85.10 40.50%

41 85

2^ 141 169 197 226 0 ' I'''' I'''' I ‘' I'''' I'''' I P’ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #211483: Nonadecane (CAS) $S n-Nonadecane 26.00 26.20 26.40 26.60 m/z 55.10 21.49%

5x3 85

I , I 113 J 141 169 197 225 268 0 r ' ' f" ' ' I ' I'' ' T' ' ' L ' ' ' ' I " ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 26.00 26.20 26.40 26.60

7110.D 5080402BB.M Mon Apr 15 17:09:18 2002 Page 11

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