GCMS surrogate recovery results, sample AE07115, April 15, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 8 Tricosane (CAS) $$ n-Tricosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

28.46 63.39 ug/L 7760800 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS'# Qual

1 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 97 2 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 3 Heptacosane 380 C27H56 000593-49-7 90 4 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 90 Abundance Scan 4320 (28.462 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85 J 28.20 28.40 28.60 28.80 0 jl^l 169 197 225 253 281 324 m/z 71.10 56.11% ii/z-> 50 100 150 200 250 300 350 Abundance #275685: Tricosane (CAS) $$ n-Tricosane 57

5000 85 28.20 28.40 28.60 28.80 m/z 43.20 42.37% .... 1 J J J J \169 211 239 267 295 324 0 f I-*! t IM r I 'I r i-i I ... I I •n/z-> 50 100 150 200 250 300 350 Abundance #211483: Nonadecane (CAS) $S n-Nonadecane 57

28.20 28.40 28.60 28.80 »Tu m/z 85.10 40.70% 85 I Oi 1 268 ■

nn/z-> 50 100 150 200 250 300 350 Abundance #320678: Heptacosane 57 28.20 28.40 28.60 28.80 m/z 55.10 21.04%

5000 85

29 J . ^69 225 253 281 309 337 380 0 ,1 ■n/z-> 50 100 150 200 250 300 350 28.20 28.40 28.60 28.80

7115.D 5080402BB.M Mon Apr 15 18:16:31 2002 Page 11

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