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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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Scanned page image, NYC-WTC_000049088
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search. Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 8 Tricosane (CAS) $$ n-Tricosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

28.46 63.39 ug/L 7760800 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 97 2 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 3 Heptacosane 380 C27H56 000593-49-7 90 4 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 90 Abundance Scan 4320 (28.462 min): 7115.D (-) m/z 57.10 100.00%| 57

5000 85

13 28’20 2840 28.60 28.807 0- t—r-r-p J ,141.169 P" 225 253 281 197 rn I I*. trPT । 11 324 m/z 71.10 56.11% m/z-> 50 100 150 200 250 300 350 Abundance #275685: Tricosane (CAS) $$ n-Tricosane 57

5000 85 ---==<J 28.20 28.40 28.60 28.80 m/z 43.20 42.37 28 I113 4A4 m/z-> 0- — 50 ,441198211239-267,295324 100 150 200 250 300 350 Abundance #211483: Nonadecane (CAS) $$ n-Nonadecane 57

28.20 28.40 28.60 28.80 5000 m/z 85.10 40.70 85

I113 141 268 0- ,1A J J J ,169197225 ■ • il' r' i r ' — ■ i ■ ■ ■ • i ■ 1 • ' i ■ miz-> 50 100 150 200 250 300 350 Abundance #320678: Heptacosane ----- ~ J P-- 57 ' • • i ■ ■'' i ‘ ‘ • i • • ■ ■ i • ■' 28.20 28.40 28.60 28.80 m/z 55.10 21.04

5000 85

291 | 1, J 1113,141 169 197 225 253 281 309 337 380 T 1 i ' "117104 1 171 r i “I r i" i 1 (■ i । । । । । ri i । i । i । T T T /z—> 50 100 150 200 250 300 350 28.20 28.40 28.60 28.80

7115.D 5080402BBC.M Tue Apr 23 15:52:57 2002 Page 11

NYC-WTC_000049088

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NYC-WTC_000049088Source: NYC Law Department, mirrored locally

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