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Sample AE10187 analysis results, May 2002

Machine-extracted title · confidence 90%

Analytical results for sample AE10187 analyzed on May 6, 2002, listing compounds detected below the method detection limit.

NYC-WTC_000082581–000082617

Folder label: “525 X 4/30/02 A 5/1/02

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Scanned page image, NYC-WTC_000082605
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10187.D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10187 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 12 Hexacosane $$ n-Hexacosane Concentration Ranlc 9

R.T. EstConc Area Relative to ISTD R.T.

22.14 0.10 ug/L 233673 Phenanthrene d-10 21.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexacosane $$ n-Hexacosane 366 C26H54 000630-01-3 80 2 Docosane (CAS) $$ n-Docosane $$ ... 310 C22H46 000629-97-0 72 3 Triacontane $$ n-Triacontane 422 C30H62 000638-68-6 72 4 Eicosane 282 C20H42 000112-95-8 72 Abundance Scan 1220 (22.142 min): 10187.D (-) m/z 57.00 100.00% 57

5000 85

113 III 155 186 214 21.80 22.00 22.20 22.40 336 m/z 71705 76776% ■n/z-> 0 4* 50 100 150 200 250 300 350 400 Abundance #311169: Hexacosane $S n-Hexacosane 57

553 85 21.80 22.00 22.20 22.40 m/z 85.05' 47716%

0 29 4-J I 1' J” J 1* J*' ' ' I ' ‘ ' ' I ' 225 253 , 295 ''' 1 i‘''' ' ''I 366 I m/z-> 50 100 150 200 250 300 350 400 Abundance#261312: Docosane (CAS) $$ n-Docosane SS C22H46 STANDARD $... 57

■'7'''.'7'7.././.: 21.80 22.00 22.20 22.40 WHBl m/z 113.15 15.99% 85

0 50 100 150 260 ' 250 ' 300 350 400 ■n/z-> Abundance 57 #343923: Triacontane $$ n-Triacontane 21.80 22.00 22:20 2240 w m/z 55.00 14.93%

5000 85

141 29 J H J \ ,^51 309 337 365 393 ^2 0 'n/z-> 50 100 150 200 250 300 350 400 21.80 22.00 22.20 22.40

10187.D 050102.M Mon May 06 15:08:11 2002 Page 14

NYC-WTC_000082605

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NYC-WTC_000082605Source: NYC Law Department, mirrored locally

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