Water quality monitoring data sheet, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\051302\11311.D Vial: 13 Acq On : 13 May 2002 9:36 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 5/10/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 14 Octacosane (CAS) $$ n-Octac... Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

22.75 0.08 ug/L 79246 Phenanthrene d-10 22.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 91 2 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 91 3 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 91 4 Eicosane 282 C20H42 000112-95-8 90 Abundance Scan 1287 (22.749 min): 11311.D (-) m/z 57.00 100.00% 57 1 85 5000

113 MMWWVMsp 22.40 22.60 22.80 23.00 0- 1 —F"L7f _L1_ • 1 i ■ ■ 188 m/z 71.00 82.62% m/z-> 50 100 150 ' 200 ' 250 300 350 400 Abundance #329269: Octacosane (CAS) $$ n-Octacosane 57

5000 85 MMVMb 22.40 22.60 22.80 23.00 11 m/z 85.05 58.12?

1113 141 169 197 225 253 281 309 394 0- • 1 i • .4 r > ■ 1 |*. 1 ifm f 11 5 1' । '1 1 1’1 1 i‘ । 1 j 1 । 1 ।

w.w. n/z-> 50 100 150 200 250 300 350 400 Abundance #245745: Heneicosane $$ n-Heneicosane 57

85 22.40 22*60 22.80 23.00 5000 m/z 55.05 22.17?

miz-> Abundance 0- 29 ।" r 50 113 A,1 1,4147 168,197,225.253 26... 100 150 ' 200 ' 250 #261311: Docosane $$ n-Docosane $$ Normal-docosane 57 300 350 400 "NYHAHwr 22.40 22*60 22.80 23*00 11 m/z 69.00 17.39% 85 5000

1 I113 4 0 +3%+ 411'l6o1,1771169,197,225,253 ‘ 281 31°. 150 ' ‘ ‘260' ' ‘ 250 ' ' 300 ' ‘ 350 ‘ ‘ 400 m/z-> 50 22.40 22:60 22.80 23.00

L1311.D 050802.M Tue May 14 11:10:45 2002 Page 16

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