GCMS sample AE07115 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 Hexadecane (CAS) $$ n-Hexad... Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

25.07 5.80 ug/L 890233 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 91 2 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 3 Eicosane (CAS) $$ n-Eicosane 282 C20H42 000112-95-8 90 4 Hexadecane 226 C16H34 000544-76-3 90 Abundance F7 Scan 3743 (25.072 min): 7115.D (-) m/z 57.10 100.00%

5000 85 AWW 4 T T T T 24.80 25.00 25.20 25.40

m/z-> 0 —* A.4.113.141.168,205.20. 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 m/z 71.10 58.23%

Abundance #154903: Hexadecane (CAS) $$ n-Hexadecane $$ Cetane 3$ n-C... 57 AAWW 85 5000 TT T T 24.80 25.00 25.20 25.40 m/z 43.10 46.16%

m/z-> 0 m 4 , J 113.141 . 169 197 226 TTDTpITmm 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 57 #245745: Heneicosane $$ n-Heneicosane MWV 85 m/z24.8085.15 25.00 25.2039.22% 25.40 5000- 41 113

m/z-> a1 15.404 1 J J 141 , 169 197 225 253 TTrf] । .4. । A. if11A । if.ixutrpi 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 1" ■,»FPTTMTIT..296 । r, ■ AWl Abundance #228982: Eicosane (CAS) $$ n-Eicosane 57 24.80 25.00 25.20 25.40 m/z 41.10 19.48%

5000 85

41 AWVw* 113 j 141 4 169 . 197 225 253 282 0 i if. I A I if 11 AI ri I 11 11 r’l 11 fl ■ 1] 1111111 n 11111 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 24.80 25.00 25.20 25.40

7115.D 5080402BBC.M Tue Apr 23 15:52:51 2002 Page 6

NYC-WTC_000049083