GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

, Data File C:\MSDCHEM\l\DATA\041002\7110.D vial: 17 Acq On 11 Apr 2002 3:12 am Operator: Bohlk Sample SAMPLE 7110 3/27/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Eicosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

28.46 17.77 ug/L ■2132650 Chrysene-dl2 30.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91 2 Hexadecane 226 C16H34 000544-76-3 90 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 4 Heptadecane (CAS) $$ n-Heptadeca... 240 C17H36 _____ 000629-78-7 90 ^ibundance Scan 4319 (28.456 min): 7110.D (-) m/z 57.10 100.00%i 7

5000 85

28.20 28.40 28.60 28.80 .169 197 225 253 324 m/z 71.10 57.20% oi ^yrrTTyYTTrp-TTTpTTTpT^^ m/z-> Abundance 20 40 60 80 100120 140160 180 200 220 240 260 280 300 320 #228992: Eicosane I 7

85 28.20 28.40 28.60 28.80 m/z 43.15 42.94% 29

m/z-> O'- ...puUUHXUJt 169 282 • I ’ " ' I " " I' * " I " " I " " I ‘ 20 40 60 80 100 120140 160180 200 220 240 260 280 300 320 ' I "' ’ I'' ’' I" '

Abundance #154905: Hexadecane 57 JI 28.20 28.40 28.60 28.80 5000 m/z 85.10 40.08%

85 29

0 ■i..l..4.'!.P....141 169 197 226 I iTl . jT. . I I . .7 I I mTj i > <1 I I I . I I r ( I > I I I ■ I I I ■ I I I ’' ” I' " ' I m/z-> Abundance 20 40 60 80 100 120 140160180 200 220 240 260 280 300 320 57 #245745: Heneicosane $$ n-Heneicosane J ■p 28.20 28.40 28.60 28.80 m/z 55.10 26734%

85 5000

UJXjWjUto 29 I 111 169 197 225 253 296 0 I. r.. I*!.. r I.. 11'... I.... I.... I... 11,, Tl/Z~> 20 40 60 80 100120140 160180 200 220 240 260 280 300 320 28.20 28.40 28.60 28.80

7110.D 5080402BB.M Mon Apr 15 17:09:21 2002 Page 13

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