GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator). Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Heneicosane $$ n-Heneicosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

30.49 68.79 ug/L 8422240 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 91 2 Eicosane 282 C20H42 000112-95-8 91 3 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 4 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 91 Abundance Scan 4666 (30.495 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85 J rm 30.20 30.40 30.60 30.80 ,j J, ■ 199, 197 225 I 267 295 352 m/z 71.10 57.42% 0 m/z-> 50 100 150 200 250 300 350 Abundance #245745; Heneicosane $5 n-Heneicosane 7

85 5000 r-r-r-r-p-TT-i 30.20 30.40 30.60 30.80

m/z-> Abundance 0 xum 50 113 ...

100 J J J , 199.197 225 253 150 200 #228992; Eicosane 250 296 300 350 m/z 43.15 41.55%

5*7

30.20 30.40 30.60 30.80 5000 m/z 85.15 40.84% 85 29 j‘*P,141 169 282 0 ' I r-y-A-rA—/—1 m/z-> 50 100 150 200 250 ' '360' 350 Abundance #211483: Nonadecane (CAS) $S n-Nonadecane 7 30.20 30.40 30.60 30.80 m/z 55.10 20.95%

5000 85

m/z-> 0 50 I J 100 150 197,225 268 250 200 300 350 30.20 30.40 30.60 30.80

7115.D 5080402BB.M Mon Apr 15 18:16:34 2002 Page 14

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