GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 12 Hexacosane $$ ri-Hexacosane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.45 64.89 ug/L 7944610 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexacosane $$ n-Hexacosane 366 C26H54 000630-01-3 95 2 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 91 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 91 4 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 Abundance Scan 4829 (31.453 min): 7115.D (-) m/z 57.10 100.00% 57

Win 85

31.20 31.40 31.60 31.80

m/z-> 0^ 44 50 J j 169 197 225 253 281 309 366 _ m/z 71.10 58.09%

Abundance #311169: Hexacosane $S n-Hexacosane 57

SEE 85 V 31.20 31.40 31.60 31.80 m/z 43.10 42.55% i 113 366 0 ■n/z-> 50 -_100____J50__200__J50_^^ Abundance #329269: Octacosane (CAS) $S n-Octacosane 57

31.20 31.40 31.60 31.80 5000 85 m/z 85.20 42.13%

394 0 m/z-> Abundance 50 5? 100 150 200 250 #245745: Heneicosane $$ n-Heneicosane 300 350 400 R 31.20 31.40 31.60 31.80 m/z 55.10 21.41%

85 5000

29 0 X JJ ......... m/z-> 50 100 150 200 250 300 350 400 31.20 31.40 31.60 31.80

7115.D 5080402BB.M Mon Apr 15 18:16:35 2002 Page 15

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