GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohllc Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 Hexadecane Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

32.38 72.98 ug/L 6741920 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexadecane 226 C16H34 000544-76-3 95 2 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 3 Pentadecane, 8-heptyl- 310 C22H46 071005-15-7 '91 4 Octacosane $$ n-Octacosane 394 C28H58 000630-02-4 91 Abundance Scan 4987 (32.381 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85 Y. 1 Ij J, 197 225 253 281 309 32.00 32.20 32.40 32.60 32.80 0^ 380 m/z 71.10 59.53% m/z-> 50 100 150 200 250 300 350 Abundance #154905: Hexadecane 57

5000 32.00 32.20 32.40 32.60 32.80 85 m/z 43.15 43.61% 29 ,113 141 169 197 226 0 m/z-> 50 100 150 200 250 300 350 Abundance #211483; Nonadecane (CAS) $S n-Nonadecane 57

32.00 32.20 32.40 32.60 32.80 5000 m/z 85.10 41.58% 85

|113 141 169 197 225 268 0 m/z-> 50 100 150 200 250 300 350 Abundance #261326: Pentadecane, 8-heptyl- . 57 32.00 32.20 32.40 32.60 32.80 m/z 55.10 21.66%

5000 85

29 210 0 ij 239 267 309 ■n/z-> 50 100 150 200 250 300 350 32.00 32.20 32.40 32.60 32.80

7115.D 5080402BB.M Mon Apr 15 18:16:36 2002 ' Page 16

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