GCMS surrogate recovery results, sample AE07115, April 15, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Librairy : C:\DATABASE\WILEY7N.L

Peak Number 14 Heptacosane Concentration Rank 6

R.T. EstConc Area . Relative to ISTD R.T.

33.27 58.95 ug/L 5445270 Perylene-dl2 34.02

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 91 2 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 91 3 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 90 4 Tricosane (CAS) $$ n-Tricosane 324 C2 3H4 8 000638-67-5 90 Abundance Scan 5139 (33.274 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85

33.00 33.20 33.40 33.60 351 394 m/z 71710 57724% 0 m/z-> 'l6o' ' 'l5o' 200 250 300 350 Abundance #320678: Heptacosane 7

J 5000 85 33.00 33.20 33.40 33.60 m/z 43710 43.14%

,1 ,PJj,''fM69.197 225 253 281 309 337 380 0 ■n/z-> 50 _J05L_-J150___200__^g__30^^ Abundance #300501: Pentacosane SS n-Pentacosane 7

33.00 33.20 33.40 33.60 5000 m/z 85.10 41.39% 85

28 |113

■n/z-> 0 u. 100 150 X 211 239 267 295 323 352 200 250 V-i^-r-T—f-T-T-T—r-r-t—p-r 300 350 Abundance #288787: Tetracosane (CAS) $$ n-Tetracosane 57 33.00 33.20 33.40 33.60 m/z55.10 20.84%

5000 85

0 I I 281 309 338 ■n/z-> 50 100 150 200 250 300 350 33.00 33.20 33.40 33.60

?115.D 5080402BB.M Mon Apr 15 18:16:38 2002 Page 17

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