GCMS sample AE07115 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 14 Heptacosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

33.27 58.95 ug/L 5445270 Perylene-d12 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptacosane 380 C27H56 000593-49-7 91 2 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 91 3 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 90 4 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 90 Abundance Scan 5139 (33.274 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85

33.00 33.20 33.40 33.60

n/z-> 0- —4 50 113 J TIP/m,ngmm/TBTTT I J 1141.1?9 197 239 267 309 351 100 150 200 394 250 300 350 m/z 71.10 57.24%

Abundance #320678: Heptacosane 57

5000 T T T 71 85 33.00 33.20 33.40 33.60 m/z 43.10 43.14% 29 J 1133,141 169 197 225 253 281 309 337 380 0- "IT ” 1 14* • 1*1 * 1 > r1 "I 1 TT 1 ■ ‘ I’ । ‘tb miz-> 50 100 150 200 250 300 350 Abundance #300501: Pentacosane $$ n-Pentacosane 57 —/—— ■4 41 ■ ■ • ■ i ■ • ■ i ’ ■ • • i ■ • ■ • 33.00 33.20 33.40 33.60 5000 m/z 85.10 41.39% 85 J

28 113 . i । 141 169

m/z-> 0- —r* 50 1 144,1+4 r"211 100 150 200 239 267 295 323 352 r rL 1 f ■ -i f i -1 r i" i > |* i i . t । 250 300 350 Abundance #288787: Tetracosane (CAS) $$ n-Tetracosane —A 57 33.00 33.20 33.40 33.60 m/z 55.10 20.84%

5000 85

। 1113 0 III 1141,169 197 225 253 281 309 338 4 1*] Ft"I f |*" i‘ i 'I r i-1 i |' i -i r । । i i i ■> । । r ri [ ■11 ■ •'11 ■1 ■' i' ■ ■ ■ i ■ • n/z—> 50 100 150 200 250 300 350 33.00 33.20 33.40 33.60

7115.D 5080402BBC.M Tue Apr 23 15:53:04 2002 Page 17

NYC-WTC_000049094