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Reference standard analysis results, sample AE10186, May 2002

Machine-extracted title · confidence 90%

Results for reference standards including hexachlorobenzene and alachlor analyzed between April 30 and May 2, 2002.

NYC-WTC_000082548–000082580

Folder label: “525 X 4/30/02 A 5/1/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohllc / Inst 213 Sample SAMPLE 10186 4/30/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Octadecane, 3-ethyl-5-(2-et... Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

20.78 0.06 ug/L 146387 Phenanthrene d-10 21.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane, 3-ethyl-5-(2-ethylbu... 366 C26H54 055282-12-7 78 2 Docosane 310 C22H46 000629-97-0 72 3 Nonane, 2-methyl- (CAS) $$ 2-Met... 142 C10H22 000871-83-0 72 4 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H3 4 000544-76-3 72 Abundance Scan 1070 (20.781 min): 10186.D (-) m/z 71.10 100.00% 71

■n/z-> 5000

0^ 45 I , *^"1 50 100 99

150 127

200 155

I.,bl.-...... 250 300 350 J.. BtVAit'l 20.40 20.60 20.80 21.00 21.20 m/z 57.05 95.49%

I Abundance #311148: Octadecane, 3-ethyl-5-(2-ethylbutyl)- (CAS) $$ 3-... 4i3

5000 71 20.40 20.60 20.80 21.00 21.20 m/z 85.10 78.13%

211 251 307 3371364 0 rI" ' 'n/z-> 50 100 150 200 250 300 350 Abundance #261313: Docosane 57

20.40 20.60 20.80 21.00 21.20 5000 85 m/z 69.05 40.17%

113 ... ,1 211,239 267 310 0 ■n/z-> 50 100 150 200 250 300 350 Abundance #38819: Nonane, 2-methyl- (CAS) $$ 2-Methylnonane $$ 2-Met... 4i3 20.40 20.60 20.80 21.00 21.20 m/z 99.05 32.84%

5000 71

98 0 15 U?' Ti/z-> 50 100 150 200 250 300 350 20.40 20,60 20.80 21.00 21.20 |

10186.D 050102.M Mon May 06 14:53:50 2002 Page 11

NYC-WTC_000082568

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NYC-WTC_000082568Source: NYC Law Department, mirrored locally

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