GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohllc Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 1-Octadecene (CAS) $$ .alph... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

26.06 29.33 ug/L 4500250 Phenanthrene-dl0 22.34

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Octadecene (CAS) $$ .alpha.-Oc... 252 C18H36 000112-88-9 97 2 1-Heptadecanol $$ n-Heptadecanol... 256 C17H36O 001454-85-9 95 3 5-Eicosene, (E)- 280 C20H40 074685-30-6 94 4 9-Eicosene, (E)- 280 C20H40 074685-29-3 94 /Xbundance Scan 3911 (26.059 min): 7115.D (-) m/z 55.10 100.00% 5fe 83

5000 111

25.80 26.00 26.20 26.40 .,.51 .11 1. 0 ___?0_ 4p_^0__ 8^ _1jg_1J0J 4gM^^ ^42 260 280 m/z 57.10 93.46% I (\bundance #190569:1-Octadecene (CAS) $$ .alpha.-Octadecene $$ Octad... 5)7 83

4

5000 111 25.80 26.00 26.20 26.40 m/z 83.10 85.42% T I 153168 196 224 ^52 i 0 ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #195644:1-Hepladecanol $$ n-Heptadecanol $S Heptadecyl al... 55 83

25.80 26.00 26.20 26.40 5000 m/z 69.10 71.82% 111 29

0 '' I' y I .lx.* I,. t, i".,, ,'l., i'. 1.1., i'..., I., I,., , i, m/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 #226374: 5-Eicosene, (E)- LA, 55 25.80 26.00 26.20 26.40 m/z 97.10 65.73% 83 5000

29 111 ..I .> 153168 196 224 252 0 -n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 25.80 26.00 26.20 26.40

7115.D 5080402BB.M Mon Apr 15 18:16:26 2002 Page 7

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