GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5O8O462BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Heneicosane Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

26.25 25.08 ug/L 3070520 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 95 2 Iron, tricarbonyl[N-(phenyl-2-py... 398 C21H14FeN203 074764-11-7 91 3 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 4 Eicosane 282 C20H42 000112-95-8 91 Abundance Scan 3943 (26.247 min): 7115.D (-) m/z 57.10 100.00% 57

aES 85

’n/z--> Abundance 0 It I i i J•168 197 225 I. n I jT. I r| r IT11 n . I [ n ri 11 r I. |i I. r j I Ti. 11.. 2O_y40_60_J0M0OJ2pj4£jl60^^ #245744; Heneicosane 253 296 I ‘” I'''' I' 26.00 26.20 26.40 26.60 m/z 71.10

1 58.91%

57

5000 85 2^00 26.20 2^40 26.60 4- m/z 43.15 44.78%

0 "T ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #331028; Iron, tricarbonyl[N-(phenyl-2-pyridinylmeUiyiene)... 57

26.00 26.20 26.40 26.60 5000 m/z 85.15 39.23% 85

41

0 22I TYrTTTYTVrTT-TTTTp-f-rTjVrT^p-rrrp'TTTpTTnrpT-TTyr^^ n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #211483: Nonadecane (CAS) $S n-Nonadecane 5(7 26.00 26.20 26.40 26.60 m/z 55.10 20780%

5000 85

1 JI J J JT. . 197 , 225 268 0 I ' ' *j ' ' ' H 'I''''I'f 'J’''•\i 'I''*II . .... rn/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 26.00 26.20 26.40 26.60

'115.D 5080402BB.M Mon Apr 15 18:16:27 2002 Page 8

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