GCMS surrogate recovery results, sample AE07110, April 15, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohlk Sample : SAMPLE 7110 3/27/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\56804d2BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Nonadecane Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

25.07 2.19 ug/L 283045 Phenanthrene-dl0 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Nonadecane 268 C19H40 000629-92-5 90 2 Iron, tricarbonyl[N-(phenyl-2-py... 398 C21H14FeN2O3 074764-11-7 83 3 Octadecane 254 C18H38 000593-45-3 83 4 Hexadecane (CAS) $$ n-Hexadecane... 226 C16H34 000544-76-3 78 Abundance Scan 3743 (25.072 min): 7110.D (-) m/z 57.10 100.00% 7

5000 85

24.80 25.00 25.20 25.40 0 m/z 71.10 55.29% " I' •'' I' ’ ‘' I' ' ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #211481: Nonadecane 7

5000 4' 85 24.80 25.00 25.20 25.40 m/z 43.10 49.50%

0 I. r.. (,. .-i 1, 11.1. rp ,T. 1.1.. f.... I. r.. I,.. 11., I r... I..,. I. t.. m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #331028; Iron, tricarbonyl[N-(phenyl-2-pyridinylmelhylene).,,

24.80 25.00 25.20 25.40 5000 m/z 85.10 36.48% 85

0 A4 .7 I 141 169 197 225 253 282 p-^rryrTTrp-rVTp'T-TTp-rT-i-p-i-rTj^ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #193178; Octadecane 57 24.80 25.00 25.20 25.40 m/z 55.10 24.37%

5000 85 4'

0 . , ,-li .1. J/, /, .. ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.80 25.00 25.20 25.40

7110.D 5080402BB.M Mon Apr 15 17:09:15 2002 Page 8

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