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GCMS analysis report for sample AE07382, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07382 for unknown compounds and surrogates conducted on April 25, 2002.

NYC-WTC_000061259–000061271

Folder label: “GCMS X 3/28/02 A 4/19/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041802\7382.D Vial: 31 Acq On : 19 Apr 2002 10:16 am Operator: Bohlk Sample : SAMPLE 7382 3/28/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N. L *★***★★***★★****★★*★★★******★**★****★★*★★***★★*★★★★*★*★★*******★***** Peak Number 3 Eicosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.07 1.95 ug/L 213844 Phenanthrene-dlO 22.34

Hit# of 5 Tentative ID MW MolForm CAS# Quai 1 Eicosane 282 C20H42 000112-95-8 90 2 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 90 3 Iron, tricarbonyl[N-(phenyl -2-py... 398 C21H14FeN2O3 074764-11-7 86 4 Pentadecane _____________________________ 212 C15H32 000629-62-9 86 Abundance Scan 3743 (25.072 min): 7382.D (-) m/z 57.10 100.00% 7

5000 85

m/z~> 0 20 XXjLm 40 113 141 60 80 100 120 140 160 180 200 220 240 260 280 24.80 25.00 25.20 25.40 m/z 71.10 57.97%

Abundance #228992: Eicosane 5(7

5000 85 24.80 25.00 25.20 25.40 4 m/z 43.20 44.78%

169 282 OUyr m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #211483: Nonadecane (CAS) $S n-Nonadecane 5(7

24.80 25.00 25.20 25.40 "m/z 85.20 39.09% 85

Okyr J .1 j J .. . 197 225240 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #331028: Iron, tricarbonyl[N-(phenyl-2-pyridinylmethylene)... 5(7 24.80 25.00 25.20 25.40 m/z 55.10 21.88%

5000 85

4

0 2^ ] m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 24.80 25.00 25.20 25.40

7382.D 5080402BBC.M Tue Apr 23 19:05:17 2002 Page 5

NYC-WTC_000061268

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NYC-WTC_000061268Source: NYC Law Department, mirrored locally

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