GCMS surrogate recovery results, sample AE07115, April 15, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 , Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Eicosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.50 68.70 ug/L 8411860 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 91 2 Nonadecane.(CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 3 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 91 4 Octacosane (CAS) $$ n-Octacosane 394 C28H58 000630-02-4 91 Abundance Scan 4496 (29.496 min); 7115.D (-) m/z 57.10 100.00% 57

5000 85

29.20 29.40 29.60 29.80 169 197 225 253 281 309 338 m/z 71.10 56.53% 0*7 I""I ■n/z-> 20 40 60 80 100120140 160 180 200 220 240 260 280 300 320 340 Abundance #228992: Eicosane

5000 -J < 85 29.20 29.40 29.60 29.80 m/z 43720 41.98% 29 il . A 169 282 0 I'''Y"''iYTr»TYTrTrpTTrp“rTT-|T^ I" I " I" " I Tl/z-> 20 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 Abundance #211483: Nonadecane (CAS) SS n-Nonadecane 57 -J ym-r- JV ■p-TT-T-

29.20 29.40 29.60 29.80 5000 m/z 85.15 39.67% 85

J TJ 169 J97 225 1 J rYTTfTpVrrfTTTVp+rTY'TTTpnVrj^^ 268 0 Ti/z-> 20 40 60 80 100 120140160 180 200 220 240 260 280 300 320 340 Abundance #261311; Docosane $$ n-Docosane $$ Normal-docosane -J 5f7 I ' ' ' ' I 29.20 29.40 29.60 29.80 m/z 55.10 21.08% 85 5000

3' 1 i J j Jj a 0 TrrrrMnMWf)TflS-p'HTfTTT^yrhTYrrTl5|TTW|^TTTYTTtTJTrT7pTT^^ ^1° 1 n/z-> 20 40 60 80 100120 140 160180 200 220 240 260 280 300 320 340 29.20 29.40 29.60 29.80

7115.D 5080402BB.M Mon Apr 15 18:16:32 2002 Page 12

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