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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\041002\7110.D vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 12 Nonadecane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.49 21.58 ug/L 2590100 Chrysene-dl2 30.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Nonadecane 268 C19H40 000629-92-5 91 2 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Heptacosane 380 C27H56 000593-49-7 90 Abundance Scan 4495 (29.490 min): 7110.D (-) m/z 57.10 100.00% 57

5000 85

29.20 29.40 29.60 29.80 ... 3! 133 141 169 196 239 267 295 338 m/z 71.10 58.76% 0- [‘4d119 M [ i i | ri T] : iT« । fl t ill J i Pi ITrI I ll 111 r J TIFIJTsuyrssTyrusasaaas m/z-> 20 40 60 80 100 120140160 180200220240260280 300320 340 Abundance #211478: Nonadecane 57

5000 85 11111,1 ‘"+* 1 'i । > 11| 11 > i 29.20 29.40 29.60 29.80 m/z 43.10 44.91% 29 i

n/z—> -7p7. ol.A —.12+141,,162,197,.725,//2F%pmppmp 20 40 60 80 100120140160 180200220240 260280 300320 340 Abundance #261311: Docosane $$ n-Docosane $$ Normal-docosane 57

85 29.20 29.40 29.60 29.80 5000 m/z 85.10 43.15%

| i 113 ...

n/z—> 0-2$4,4.4..444,169,+,19,7,225,,253281.,310, 20 40 60 80 100120140160180 200 220 240 260 280 300 320 340 Abundance #228992: Eicosane — 57 T TT T T 29.20 29.40 29.60 29.80 m/z 55.10 22.35%

5000 85 29

m/z—> 4A.41144.141..169 282 20 40 60 80 100120140160180200220240260280 300 320 340 29.20 29.40 29.60 29.80

7110.D 5080402BBC.M Tue Apr 23 15:52:21 2002 Page 14

NYC-WTC_000049053

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NYC-WTC_000049053Source: NYC Law Department, mirrored locally

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