GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst Instrumen Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscah Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Docosane (CAS) $$ n-Docosan... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

27.38 48.61 ug/L 5952230 Chrysene-dl2 30.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane (CAS) $$ n-Docosane $$ ... 310 C22H46 000629-97-0 97 2 Docosane 310 C22H46 000629-97-0 95 3 Nonadecane (CAS) $$ n-Nonadecane 268 C19H40 000629-92-5 91 4 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 90 Abundance Scan 4136 (27.381 min): 7115.D (-) m/z 57.10 100.00% 7

I 5000 85

27.00 27.20 27.40 27.60 27.80 . .y..1^... .1^.. 253 281 310 m/z 71.10 56.09% 0 -TrrTTn-rT-pTTVp-rrTj-TTT-rpTTTyrTTTpnTTyTT^^ m/z-> 40 60 80 100 120 140 160 180200 220 240 260 280300 Abundance#261317; Docosane (CAS) $S n-Docosane $S C22H46 STANDARD $... 5'7 (1 85 5000 27.00 27.20 27.40 27.60 27.80 m/z 43.15 42.49%

m/z-> 0 UXuXiX 40 60 80 100 120 140 160 180 200 220 240 260 280 300 310.

Abundance ’ #261313: Docosane 5?

27.00 27.20 27.40 27.60 27.80 5000 85 m/z 85.15 39.80%

41 113 141 ITi rl| ifl I {1 1 J J , 211 , 239 267 310 0 I . .T, I I . , , I , . , , t. . 1*1 . 1 l| , I I . , . , , . I'. I , , , , , m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #211483: Nonadecane (CAS) $S n-Nonadecane 7 27.00 27.20 27.40 27.60 27.80 m/z55.10 19.83%

5000 85 I

Tl/z-> 0 u 40 60 80 100 120 140 160 180 200 220 240 260 280 300 268 27.00 27.20 27.40 27.60 27.80

7115.D 5080402BB.M Mon Apr 15 18:16:28 2002 Page 9

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