Sample AE10187 analysis results, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10187.D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohlk / Inst 213 Sample STkMPLE 10187 4/30/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 9 Docosane $$ n-Docosane $$ N... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

20.78 0.13 ug/L 279232 Phenanthrene d-10 21.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 64 2 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 64 3 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 64 4 Tridecane, 1-iodo- (CAS) $$ 1 IO... 310 C13H27I 035599-77-0 53 Abundance Scan 1070 (20.781 min): 10187.D (-) m/z 71.10 100.00% 71

5000 113 155 135 20.40 20.60 20.80 21.00 21.20 286 II m/z 85.20 74.93% 0 nn/z-> 50 100 150 200 250 300 350 Abundance #261311: Docosane $S n-Docosane $S Normal-docosane 5l7

85 5000 20.40 20.60 20.80 21.00 21.20 m/z 57.10 70.33%

m/z-> Abundance 0 JKux 50 100 150 200 250 253 281 310 <—f-T-T—I—I—t—I

#300501; Pentacosane $S n-Pentacosane 300 350 7

20.40 20.60 20.80 21.00 21.20 TQM m/z 113.10 26.96% 85

28 Il 141 i I 1 i i J i J .J.’'?^.18£| 211 239 267 295 323 3^2 Qi Tl/z-> 50 100 150 200 250 300 350 Abundance #275685: Tricosane (CAS) $S n-Tricosane 7 20.40 20.60 20.80 21.00 21.20 m/z 99.20 25.75%

5000 85

'n/z-> 0 50 100 150 211 239 267 295 324 200 250 300 350 Mw.... 20.40 20,60 20.80 21.00 21.20

10187.D 050102.M Mon May 06 15:08:08 2002 Page 11

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