NYC-WTC_000057993
Instrument sequence log detailing the order of analysis for calibration standards and environmental samples in December 2001.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗Analytical results for organic compounds including hexachlorobenzene and EPTC using Method 525.2 in early May 2002.
NYC-WTC_000082469–000082494Folder label: “525 X 4/30/02 A 5/1/02”

OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Response Factor Report Instrumen
Method : C;\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon May 06 12:42:26 2002 Response via : Initial Calibration
Calibration Files 2 =C02A0501.D 3 =C05A0501.D 4 =C1AO5O1.D 5 =C2A0501.D 6 =C5A0501.D 7 ■ =C10A0501.D
Compound 2 3 4 5 6 7 Avg %RSD
1) I Acenaphthene-dlO -------------istd-------------- 2) S 1,3-Dimethyl-2- 0.246.0.238 0.240 0.237 0.224 0.206 0.229 5.60 3) Hexachlorocyclo 0.049 0.075 0.078 0.129 0.142 0.120 38.59 4) Hexachlorobenze 0.322 0.334 0.325 0.319 0.301 0.312 4.87 5) EPTC 0.319 0.412 0.419 0.472 0.485 0.446 13.57 6) 2,6-Dinitrotolu 0.078 0.111 0.194 0.230 0.198 37.84 7) 2,4-Dinitotolue 0.024 0.055 0.162 0.237 0.188 59.20 8) Molinate 0.505 0.610 0.605 0.716 0.720 0.670 12.94
9) I Phenanthrene d-10 ------- ISTD---------------- 10) Simazine 0.042 0.068 0.116 0.133 0.112 36.47 11) Atrazine 0.157 0.187 0.210 0.218 0.211 14.13 12) Alachlor 0.199 0.239 0.226 0.230 0.229 6.80 13) Terbacil 0.027 0.053 0.090 0.104 0.089 39.93 14) Acetochlor 0.113 0.149 0.161 0.172 0.162 15.16 15) Metribuzin 0.076 0.137 0.222 0.245 0.211 35.50 — 16) Metolachlor 0.474 0.615 0.690 0.723 0.682 15.63 17) Butachlor 0.104 0.139 0.179 0.200 0.178 23.34 18) 4,4'-DDE 0.181 0.215 0.209 0.211 0.208 6.50
19) I Chrysene d-12 ------------------------- istd---------------------------- 20) S Triphenyl Phosp 0.177 0.182 0.211 0.220 0.236 0.241 0.223 17.99 21) S Perylene D-12 0.627 0.612 0.639 0.690 0.738 0.705 0.696 11.86 22) Bis (2-Ethylhex 0.217 0.296 0.536 0.693 0.614 44.54 23) Bis (2-Ethylhex 0.386 0.558 0.956 1.111 1.005 39.44 24) Benzo (a) pyren 0.126 0.167 0.264 0.409 0.813 0.927 0.618 71.23
25) I p-Terphenyl d-14 -------------istd---------------- 26) S Acenaphthene d- 0.000 0.000 0.000 0.000 0.000 7.427 0.743 E5 316.22 27) S Phenanthrene d- 0.000 0.000 0.000 0.000 0.000 1.017 0.102 E6 316.22 28) S Chrysene d-12 ( 0.000 0.000 0.000 0.000 0.000 6.783 0.678 E5 316.22
(#) = Out of Range ### Number of calibration levels exceeded format ### 050102.M . Mon May 06 12:44:40 2002 Page 1
NYC-WTC_000082469
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NYC-WTC_000057993
Instrument sequence log detailing the order of analysis for calibration standards and environmental samples in December 2001.
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Chromatographic data file from May 28, 2002 showing instrument analysis of DFTPP and Endrin standards.
1 shared topics · similarity 0.993
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Log sheet recording laboratory sample numbers, processing times, and final volumes for samples analyzed in mid-December 2001.
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Raw analytical data file containing a total ion chromatogram generated on April 4, 2002, using AcqMethod 508SCAN.
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DFTPP mass spectral limit results showing all parameters passed on April 12, 2002.
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Fragmented header page from a GCMS document batch dated May 2002 showing Method 508.
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Quality control spiked sample analysis for pesticide testing method 525.2, completed June 28, 2002, with recovery percentages for known pesticide analytes.
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Laboratory report documenting GCMS analysis of environmental sample AE06095 conducted on April 18, 2002.
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Laboratory report documenting GCMS analysis of sample AE07380 for unknown compounds conducted on April 25, 2002.
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Laboratory report showing GCMS analysis of environmental sample AE03258 on April 3, 2002 with surrogate recovery data.
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Laboratory report documenting GCMS analysis of environmental sample AE03260 conducted on April 3, 2002.
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NYC-WTC_000082458
Fragmented DEP document from the World Trade Center site dated April 30 to May 1, 2002.
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NYC-WTC_000082459
Form recording drip rate and pH measurements for water samples analyzed in late April to early May 2002.
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NYC-WTC_000082464
Chromatogram and instrument log from May 1, 2002, displaying abundance data for DFTPP and endrin compounds.
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NYC-WTC_000082495
Analytical results for organic compounds including hexachlorobenzene and EPTC using Method 525.2 in early May 2002.
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NYC-WTC_000082497
Results for DFTPP and endrin internal standards from sample AE10186 analyzed on May 2, 2002.
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