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← Document results/DEP Box 65/525 X 4/30/02 A 5/1/02
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Method 525.2 compound analysis results, May 2002

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Analytical results for organic compounds including hexachlorobenzene and EPTC using Method 525.2 in early May 2002.

NYC-WTC_000082469–000082494

Folder label: “525 X 4/30/02 A 5/1/02

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NYC 9/11 Public Portal Document

Response Factor Report Instrumen

Method : C;\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon May 06 12:42:26 2002 Response via : Initial Calibration

Calibration Files 2 =C02A0501.D 3 =C05A0501.D 4 =C1AO5O1.D 5 =C2A0501.D 6 =C5A0501.D 7 ■ =C10A0501.D

Compound 2 3 4 5 6 7 Avg %RSD

1) I Acenaphthene-dlO -------------istd-------------- 2) S 1,3-Dimethyl-2- 0.246.0.238 0.240 0.237 0.224 0.206 0.229 5.60 3) Hexachlorocyclo 0.049 0.075 0.078 0.129 0.142 0.120 38.59 4) Hexachlorobenze 0.322 0.334 0.325 0.319 0.301 0.312 4.87 5) EPTC 0.319 0.412 0.419 0.472 0.485 0.446 13.57 6) 2,6-Dinitrotolu 0.078 0.111 0.194 0.230 0.198 37.84 7) 2,4-Dinitotolue 0.024 0.055 0.162 0.237 0.188 59.20 8) Molinate 0.505 0.610 0.605 0.716 0.720 0.670 12.94

9) I Phenanthrene d-10 ------- ISTD---------------- 10) Simazine 0.042 0.068 0.116 0.133 0.112 36.47 11) Atrazine 0.157 0.187 0.210 0.218 0.211 14.13 12) Alachlor 0.199 0.239 0.226 0.230 0.229 6.80 13) Terbacil 0.027 0.053 0.090 0.104 0.089 39.93 14) Acetochlor 0.113 0.149 0.161 0.172 0.162 15.16 15) Metribuzin 0.076 0.137 0.222 0.245 0.211 35.50 — 16) Metolachlor 0.474 0.615 0.690 0.723 0.682 15.63 17) Butachlor 0.104 0.139 0.179 0.200 0.178 23.34 18) 4,4'-DDE 0.181 0.215 0.209 0.211 0.208 6.50

19) I Chrysene d-12 ------------------------- istd---------------------------- 20) S Triphenyl Phosp 0.177 0.182 0.211 0.220 0.236 0.241 0.223 17.99 21) S Perylene D-12 0.627 0.612 0.639 0.690 0.738 0.705 0.696 11.86 22) Bis (2-Ethylhex 0.217 0.296 0.536 0.693 0.614 44.54 23) Bis (2-Ethylhex 0.386 0.558 0.956 1.111 1.005 39.44 24) Benzo (a) pyren 0.126 0.167 0.264 0.409 0.813 0.927 0.618 71.23

25) I p-Terphenyl d-14 -------------istd---------------- 26) S Acenaphthene d- 0.000 0.000 0.000 0.000 0.000 7.427 0.743 E5 316.22 27) S Phenanthrene d- 0.000 0.000 0.000 0.000 0.000 1.017 0.102 E6 316.22 28) S Chrysene d-12 ( 0.000 0.000 0.000 0.000 0.000 6.783 0.678 E5 316.22

(#) = Out of Range ### Number of calibration levels exceeded format ### 050102.M . Mon May 06 12:44:40 2002 Page 1

NYC-WTC_000082469

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