Reference standard analysis results, sample AE10186, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

. Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10186 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Heptadecane, 9-octyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

18.40 0.17 ug/L 345970 Acenaphthene-dl0 17.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 72 2 Docosane $$ n-Docosane $$ Normal... 310 C22H46 000629-97-0 64 3 Tetracosane (CAS) $$ n-Tetracosane 338 C24H50 000646-31-1 64 4 Pentacosane $$ n-Pentacosane 352 C25H52 000629-99-2 59 <kbundance Scan 807 (18.396 min); 10186.D (-) “m/z 85.00 100.00% 85 57

113

................................... wXw 18.00 18.20 18.40 18.60 18.80 m/z 71.10 89.51% O! " I" " I" " I" " I"'' I" •' I" " I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340

AuJVjv Abundance #300498; Heptadecane, 9-octyl-

lililili 85 18.00 18.20 18.40 18.60 18.80 m/z 57.10 82.57%

m/z-> 0 4 40 60 80 100120140160180 200220 240260 280 300 320 340 Abundance #261311: Docosane $S n-Docosane $S Normal-docosane 57 7 ,-rr: ,~7 85 18.00 18.20 18.40 18.60 18.80 5000 m/z 55.00 34.05%

3 0 ■n/z-> 40 60 80 100120140160180200220 240260 280 300 320 340 Abundance #288787; Tetracosane (CAS) $$ n-Tetracosane 57 18.00 18.20 18.40 18.60 18.80 m/z 69.00 30.52%

TiTiTil 85

I 113 0 rr ,, I , ,I , , IpI, , ■, m.I ,p m/2-> 40 "60 80 1001 'l40' 160 180 200 220 240 260 2^' 300 320 340 ' 18.00 18.20 18.40 18.60 18.80

10186.D 050102.M Mon May 06 14:53:48 2002 Page 9

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