Reference standard analysis results, sample AE10186, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10186 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Tetracosane $$ n-Tetracosane Concentration Rank 13

R.T. EstConc Area Relative to ISTO R.T.

18.55 0.07 ug/L 147726 Acenaphthene-dl0 17.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane $$ n-Tetracosane 338 C24H50 000646-31-1 43 2 Eicosane (CAS) $$ n-Eicosane 282 C20H42 000112-95-8 35 3 Tridecane, 1-iodo- $$ Tridecyl i... 310 C13H27I 035599-77-0 27 4 4-Tetradecanone 212 C14H28O 026496-20-8 22 flibundance Scan 824 (18.550 min): 10186.D (-) m/z 71.15 100.00% 71

162 5000 111

4 iMlw 5: 30 210 18.20 18.40 18.60 18.80 0 Jj I" " r I" " I' •" I " '' I "m/z 57.05 7472?% Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 /Abundance #288782: Tetracosane $S n-Tefracosane 57

Saw 85 ■TT 18.20 18.40 18.60 18.80 m/z 85.10 68.63% 29 113 I I u !1u1L^2L35I.2813O9^^ 0 Tp-rrqVrTtpTVr|-rnTY’"r/TjTWT^TTTTpT^ m/z-> 20 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 Abundance #228991: Eicosane (CAS) $S n-Eicosane

18.20 18.40 18.60 18.80 85 m/z 162.20 63.71% 5000

29 I 155 183 225 0 VryrrT- T"' ‘ I m/z-> 20 40 60 80 100120140160180 200 220 240 260 280 300 320 340 Abundance #260094: Tridecane. 1-iodo- $$ Tridecyl iodide ' I ' ' ' ' I > < ' I I I I I I I I " 5(7 18.20 18.40 18.60 18.80 m/z 164.10 48.91%

5000 85

28 113 0 310 F I " I . I . . I . I "-I . I . • . • I H n/2--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 18.20 18.40 18.60 18.80

10186.D 050102.M • Mon May 06 14:53:49 2002 Page 10

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