Sample AE10187 analysis results, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10187.D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10187 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 4,4-Dimethylcyclooctene Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

18.56 0.09 ug/L 177774 Acenaphthene-dl0 17.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4,4-Dimethylcyclooctene 138 C10H18 000000-00-0 43 2 2-ETHYL-2',2',2'-D3-CYCLOPENTANONE 115 C7H9D3O 032454-48-1 38 3 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 35 4 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 35 Abundance Scan 825 (18.559 min): 10187.D (-) m/z 85.10 100.00% 8(5

57

5000

I I I T “T

•n/z-> 0 WmjIjXiMt 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 205 rp-TT p ni I.... I.... I 322 I 18.20 18.40 18.60 18.80 m/z 57.00 71.67%

Abundance #34435: 4,4-Dimethylcyciooctene 5f7 85

553 18.20 18.40 18.60 18.80 m/z 71.05 70.50%

127 0 rM- Ti/z-> 20 40 60 80 100120 140160 180 200 220 240 260 280 300 320 Abundance #13414: 2-ETHYL-2',2',2'-D3-CYCLOPENTANONE 85

59 18.20 18.40 18.60 18.80 5000 m/z 99.00 31.02%

41 115 I m/z-> 0 w* I ' H I I .I .• I I I. .I 20 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 Abundance #113302: Tetradecane (CAS) $$ n-Tetradecane SS Isotetradecane I""I""I

43 18.20 18.40 18.60 18.80 m/z 83.00 27.81%

5000 71

■n/z-> 0 4 ■I J y . 155 198 I" ’ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 . 18.20 18.40 18.60 18.80

.0187.D 050102.M Mon May 06 15:08:05 2002 Page 8

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