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Reference standard analysis results, sample AE10186, May 2002

Machine-extracted title · confidence 90%

Results for reference standards including hexachlorobenzene and alachlor analyzed between April 30 and May 2, 2002.

NYC-WTC_000082548–000082580

Folder label: “525 X 4/30/02 A 5/1/02

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Scanned page image, NYC-WTC_000082555
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10186 4/30/02 inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Hexacosane $$ n-Hexacosane Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

14.21 0.08 ug/L 159650 Acenaphthene-dl0 17.59

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexacosane $$ n-Hexacosane 366 C26H54 000630-01-3 80 2 Tricosane (CAS) $$ n-Tricosane 324 C23H48 000638-67-5 72 3 Heneicosane $$ n-Heneicosane 296 C21H44 000629-94-7 72 4 Undecane, 3,8-dimethyl- 184 C13H28 _______ 017301-30-3 64 Abundance Scan 345 (14.205 min); 10186.D (-) m/z 57.10 100.00% 57 85

5000

113 , 1 169 13.80 14.00 14.20 14.40 14.60 371 436 n/z-> 0^ 41 A ,1 I 50 100 11 III I 150 2OO 25O 300 350'400 m/z 71.05 94.57%

Abundance #311169; Hexacosane $S n-Hexacosane 5*7

5000 85 13.80 14.00 14.20 14.40 14.60 m/z 85.10 76.58%

m/z-> oi

Abundance

5000 50 5*7 100

85 150 200 250 300 #275685; Tricosane (CAS) $S n-Tricosane 350 400

w 13.80 14.00 14.20 14.40 14.60 m/z 70.10 32.67%

113 28 Jn^169 211 239 267 295 324 0^ A 250 ' ' 300 350 400 ■n/z-> 50 100 150 200 Abundance #245745; Heneicosane $$ n-Heneicosane 517 13.80 14.00 14.20 14.40 14.60 m/z 84.10 26.50%

85

29 i j J,I J /f\^9lg7 225 253 296 0 ■n/z-> 50 100 150 200 250 300 350 400 13.80 14.00 14.20 14.40 14.60

10186.D 050102.M Mon May 06,14:53:41 2002 Page 3

NYC-WTC_000082555

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NYC-WTC_000082555Source: NYC Law Department, mirrored locally

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