Reference standard analysis results, sample AE10186, May 2002

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Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10186 4/30/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 3-Ethyl-3-methylheptane $$ ... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

15.01 0,07 ug/L 155446 Acenaphthene-dl0 17.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Ethyl-3-methylheptane $$ Hepta... 142 C10H22 017302-01-1.50 2 2-Bromononane $$ sec-Nonyl bromi... 206 C9H19Br . 002216-35-5 50 3 Eicosane 282 C20H42 000112-95-8 47 4 pentadecane _______________________ 212 C15H32 000629-62-9 35 Abundance Scan 434 (15.013 min): 10186.D (-) m/z 71.10 100.00% 7(1

5000

127 14.60 14.80 15.00 15.20 15.40

m/z-> 04- 0 50 100 150 ...... X 200 250 300 350 m/z 57.05 69.44%

Abundance #38900: 3-Ethyl-3-methylheptane $$ Heptane. 3-ethyl-3-methyl-

85

5000 113 14.60 14.80 15.00 15.20 15.40 29 m/z 85.05 62.10%

04 rn/z-> 0 50 100 150 200 250 300 350 Abundance #123200: 2-3romononane S$ sec-Nonyl bromide $S Nonane, 2-b... 43 71

14.60 14.80 15.00 15.20 15.40 m/z 55.00 31.43% itiliBI

.n,127

Tl/z-> 0 0 "1 50 , 107^ I, 149.......... . 100 150 200 250 300 350 Abundance #228992; Eicosane 57 M^eo 14.80 15.00 1^20 15.40 m/z84.00 24.16%

5000 85 29 I ,141 169 282 04 m/z-> 0 50 100 150 200 250 300 350 14.60 14,80 15.00 15.20 15.40

.0186.D 050102.M Mon May 06 14:53:42 2002 Page 4

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