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Sample AE10187 analysis results, May 2002

Machine-extracted title · confidence 90%

Analytical results for sample AE10187 analyzed on May 6, 2002, listing compounds detected below the method detection limit.

NYC-WTC_000082581–000082617

Folder label: “525 X 4/30/02 A 5/1/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\10187.D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10187 4/30/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 (.beta.R*,.gamma.R*(S*))-.a... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

17.23 0.09 ug/L 179856 Acenaphthene-dlO 17.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 (.beta.R*,.gamma.R*(S*))-.alpha.... 378 C24H26O2S 073089-61-9 22 2 Ethanone, 1-(3,4-dimethoxyphenyl)- 180 C10H12O3 001131-62-0 14 3 Silane, trimethyl(4-methylphenox... 180 C10H16OSi 017902-32-8 14 4 Ethanone, 1-(3,4-dimethoxyphenyl)- 180 C10H1203 001131-62-0 14 Wjundance Scan 679 (17.235 min): 10187.D (-) m/z 57.00 100.00% 57 165

91 180 205 5000 109 135 220 17.00 17.20 17.40 17.60

Tl/Z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 uUo- I I 290 m/z 165.10 87.16%

Abundance #319396: (.beta.R*,.gamma.R*(S’))-,alpha.,.alpha.-Dimethyi... 140 205 91 220

5000 I 123 17.00 17.20 17.40 17.60 165 m/z 205.10 56.11% 238 I 262 Olyr I i ' 'I'''' I'' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #86184: Ethanone, 1-(3,4-dimethoxyphenyl)- 165

180 17.00 17.20 17.40 17.60 5000 m/z 91.10 55.74%

. 77 137 27 ,h 6g li „ ■'22 0 m/z-> '\bundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 #86476: Silane, trimethyl(4-methylphenoxy)- $$ Silane, tri... 1^5 WOO17.00 17.20 17.40 17.60 m/z 180.20 51.97%

5000 180

91 135

M 73 42 111 109 [ 150 , oV I. . I I , .TJ . I'''' I 11" • I' 1111 ' ' ' I ' ' Ti/z-> 20 406080 100 120 140 160 180 200 220 240 260 280 17,00 17.20 17.40 17.60

10187.D 050102.M Mon May 06 15:08:00 2002 Page 4

NYC-WTC_000082595

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NYC-WTC_000082595Source: NYC Law Department, mirrored locally

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