Results for reference standards including hexachlorobenzene and alachlor analyzed between April 30 and May 2, 2002.
NYC-WTC_000082548–000082580Folder label: “525 X 4/30/02 A 5/1/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\l\DATA\050202\10186.D Vial: 22 Acq On 2 May 2002 6:59 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10186 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2,6-DI-T-BUTYL-4-METHYLENE-... Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
17.46 0.08 ug/L 173105 Acenaphthene-dl0 17.59
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2,6-DI-T-BUTYL-4-METHYLENE-2,5-C... 218 C15H22O 002607-52-5 90 2 2,6-DI-T-BUTYL-4-METHYLENE-2,5-C... 218 C15H22O 002607-52-5 50 3 3-[4'-(t-Butyl)-2'-methylphenyl]... 218 C15H22O 000000-00-0 47 4 ls,4R,7R,llR-l,3,4,7-Tetramethyl... 218 C15H22O 000000-00-0 35 Abundance Scan 704 (17.462 min): 10186.D (-) m/z 161.10 100.00% 1$1
5000 203 175 55 77 91 105 119^^147 218 189 17.20 17.40 17.60 17.80 l|i |i il I l|i|i (Hl I Illi II I 4 ly-XL-ry k-rjp-T m/z-> 20 0 puJW 40 60 80 100 120 140 160 180 200 220 m/z 203.20 48.13%
Abundance#141826: 2,6-DI-T-BUTYL-4-METHYLENE-2.5-CYCLOHEXADIENE-1-O l6l 203 218
175 17.20 17.40 17.60 17.80 41 80 189 m/z 175.20 34.80% 57 105 121 145 0 15^24, JXIJUJU ' ' ' ' I ' ' ' ’ I ' ' ' ' I ' ' ' ' I ■n/z-> 20 40 60 80 100 120 140 160 180 200 220- Abundance#141825: 2.6-Dl-T-BU'rYL-4-METHYLENE-2,5-CYCLOHEXADIENE-1-O 161 ___ ,,, I jV', I I I (|\ //^, , , I I I , I,,
203 17.20 17.40 17.60 17.80 iililil m/z 163.20 25.96% 91 175 218 77 55 ”^128 147 189
m/z-> 0 20 40 I Nil, 60 80 iXOjLi 100 120 II, ,1, 140 160 180 200 220 P ' I
Abundance #142129; 3-[4'-(t-Butyl)-2'-methylphenyl]-2-methylpropanal l6l I ‘ ' I 17.20 17.40 17.60 17.80 m/z 162.20 2^793% 203 5000
131 145 218
■n/z-> 0 20 41 I I 40 57
'eO 7 T TT I 80 ioo' 120 140 160 I 180 200 220 17.20 17.40 17.60 17.80
10186.D 050102.M Mon May 06 14:53:45 2002 Page 6
NYC-WTC_000082558
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NYC-WTC_000082581
Analytical results for sample AE10187 analyzed on May 6, 2002, listing compounds detected below the method detection limit.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000082518
Results for laboratory blank sample AE10186 analyzed between April 30 and May 2, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.989
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000015919
Form recording water quality parameters including drip rate, pH, and volume for samples analyzed in mid-May 2002.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012615
Laboratory report showing analytical results for pesticides and related compounds with values below method reporting limits.
1 shared non-person entities · 1 shared topics · similarity 0.990
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016024
Blank analysis for sample AE11755 to verify absence of contamination in laboratory equipment and procedures, completed May 13, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.988
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049027
Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049063
Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.
1 shared topics · similarity 0.986
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000061033
Laboratory report listing GCMS analysis of deuterated surrogates for sample AE07110 on April 15, 2002.
1 shared topics · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004935
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared topics · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011027
Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02720 including surrogate recovery.
1 shared topics · similarity 0.983
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025102
Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000061112
Laboratory report listing GCMS analysis of surrogates for sample AE07115 on April 15, 2002.
1 shared topics · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000082458
Fragmented DEP document from the World Trade Center site dated April 30 to May 1, 2002.
Filed in the same folder
NYC-WTC_000082459
Form recording drip rate and pH measurements for water samples analyzed in late April to early May 2002.
Filed in the same folder
NYC-WTC_000082464
Chromatogram and instrument log from May 1, 2002, displaying abundance data for DFTPP and endrin compounds.
Filed in the same folder
NYC-WTC_000082469
Analytical results for organic compounds including hexachlorobenzene and EPTC using Method 525.2 in early May 2002.
Filed in the same folder
NYC-WTC_000082495
Analytical results for organic compounds including hexachlorobenzene and EPTC using Method 525.2 in early May 2002.
Filed in the same folder