Laboratory blank analysis results, sample AE10186, May 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050202\LBA0502.D Vial: 18 Acg On 2 May 2002 3:53 pm Operator: Bohlk / Inst 213 Sample LB 4/30/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peale Number 1 Phenol, 2,6-bis(1,1-dimethy... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

17.95 4.43 ug/L 8601850 Acenaphthene-dlO 17.59

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenol, 2,6-bis(1,1-dimethylethy... 220 C15H24O 000128-37-0 98 2 Phenol, 2,6-bis(1,1-dimethylethy... 220 C15H24O 000128-37-0 98 3 BUTYL HYDROXY TOLUENE 220 C15H24O 000128-37-0 98 4 Butylated Hydroxytoluene $$ Phen... 220 C15H24O 000128-37-0 98 Abundance Scan 758 (17.951 min): LBA0502.D (-) m/z 205.20 100.00% 2(115

5000

57 220 81 , IOS , 129 I 161 V 17.60 17.80 18.00 18.20 0 246 -p-m-j- 289 m/z 220.20 22.49% m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #144849: Phenol, 2.6-bis(1,1-dimethylethyl)-4-methyl- (CAS... 2(1)5

57 17.60 17.80 18.00 18.20 220 m/z 57.10 17.83% 41 81 195121 ^1^16117 • If I . II ID , I , I, I I 0 ' T ” " I r' I ' • I ' ' ' ' I ' I I I I I I'l I I P" ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #144850; Phenol, 2,6-bis(1,1-dimethylethyl)-4-methyl- (CAS... 2()5

■i(i|tTvr|Tirr|i 17.60 17.80 18.00 18.20 5000 m/z 206.20 16.05%

220

.0 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #145122: BUTYL HYDROXY TOLUENE 2(115 17.60 17'so m/z 145.10 14.26%

57 220 145 41 177 81 128 161 I 0 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 17.60 17.80 18.00 18.20

LBA0502.D 050102.M Mon May 06 14:19:52 2002 Page 3

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