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Pesticide analysis results, sample AE11755, May 2002

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Laboratory report listing pesticide and organic compound concentrations in sample AE11755 analyzed between May 10 and May 13, 2002.

NYC-WTC_000015992–000016005

Folder label: “525 X 5/10/02 A 5/13/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\LBB0513.D Vial: 12 . Acg On : 13 May 2002 8:50 pm Operator: Bohlk / Inst 213 Sample : LB 5/13/02 Inst : Instrumen Mise : Multipir: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Phenol, 2,6-bis(1,1-dimethy... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

18.55 0.80 ug/L 638946 Acenaphthene -dl0 18.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenol, 2,6-bis(1,1-dimethylethy... 220 C15H24O 000128-37-0 98 2 Phenol, 2,6-bis(1,1-dimethylethy... 220 C15H240 000128-37-0 98 3 Phenol, 2,6-bis(1,1-dimethylethy... 220 C15H24O 000128-37-0 98 4 BUTYL HYDROXY TOLUENE 220 C15H240 000128-37-0 98 Abundance Scan 824 (18.550 min): LBB0513.D (-) m/z 205.20 100.00% 205

5000

220 57 145 18.20 18.40 18.60 18.80 0- -IP$2 31,22 /05,112131/1,11.177189,1 L m/z 220.20 22.58% m/z-> 40 60 80 100 120 140 160 180 200 220 Abundance #144849: Phenol, 2,6-bis(1,1-dimethylethyl)-4-methyl- (CAS... 205

5000 57 18.20 18.40 18.60 18.80' T 220 m/z 57.10 17.26% 41 145 69 91 105 119 131 | 161 177189 I 0- It ,, r . t, 2 * ,,1.1 V i*, . I, — Tl/Z-> 40 60 80 100 120 140 160 180 200 220 Abundance #144850: Phenol, 2,6-bis(1,1-dimethylethyl)-4-methyl- (CAS... 205 +A4A 18.20 18.40 18.60 18.80 5000 m/z 206.20 17.01%

220 57 41 | 77 91 105 119 133145 161 177 189 I 0--- n/z-> 40 60 80 100 120 140 160 180 200 220 Abundance #144843: Phenol, 2,6-bis(1,1-dimethylethyi)-4-methyl- (CAS... 205 18.20 18.40 18.60 18.80 ' P m/z 145.10 14.09%

5000

57 220 41

m/z—> 1s9 81 93 105 119 131140115 160 0k^ * » r | I TT 11 1 1 T“TI 40 60 80 100 120 161 177189 * r r‘ ■ '/i । 188 7gTd 180 200 220 18.20 18.40 18.60 18.80

BB0513.D 050802.M Tue May 14 11:03:05 2002 Page 3

NYC-WTC_000016001

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NYC-WTC_000016001Source: NYC Law Department, mirrored locally

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GCMS blank results, April 2002 · Box DEP Box 57

NYC-WTC_000060990

Gas chromatography mass spectrometry blank analysis report showing non-detect levels for various organic compounds.

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