Laboratory blank analysis results, sample AE11755, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051302\LBA0513 .D Vial: 8 • Acq On : 13 May 2002 5:46 pm Operator: Bohlk / Inst 213 Sample : LB 5/10/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L

Peak Number 6 Eicosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

18.30 0.10 ug/L 78981 Acenaphthene-dl0 18.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8 78 2 Heptadecane 240 C17H36 000629-78-7 78 3 Tricosane 324 C23H48 000638-67-5 72 4 Dodecane, 1-iodo- 296 C12H25I 004292-19-7 72 Abundance Scan 796 (18.296 min): LBA0513.D (-) m/z 71.10 100.00% 71

5000 99 127 155 TT-p-T A A ' ‘ 1’’’ 1 1 1 1 18.00 18.20 18.40 18.60 49 0- 1.................................... n 11 ri 111111111111 n 11 j11UUTIT TT rr m/z 57.10 84.06% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #228984: Eicosane 57

5000 " I " nA ■ d • I ■ ■ 85 18.00 18.20 18.40 18.60 29 m/z 85.10 67.82%

1 4 ., 113 A 141.169 197 225 253 ...... ... 0- . v.. p. .-r,. ri > > q ■ ■ y ■ । n । ■ f 11 it । > r r > p > > r| TTetl > ■ > > । > ■ < > i ■ ITTTrTTu m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #174548: Heptadecane 57 _AA 18.00 18.20 18.40 18.60 5000 m/z 99.10 31.03% 85 29

m/z—> 0- ,4.,4.1.+141.,16 197 240 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #275686: Tricosane 43 18.00 18.20 18.40 18.60 m/z 55.10 26.35% 71 5000

99 I I 155 183 211 253 281 J J j 127 324 0-mmtIEugmupgTu -AA 11'1 /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 18.00 18.20 18.40 18.60

BA0513.D 050802.M Tue May 14 10:36:10 2002 Page 8

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