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Pesticide analysis results, sample AE11755, May 2002

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Laboratory report listing pesticide and organic compound concentrations in sample AE11755 analyzed between May 10 and May 13, 2002.

NYC-WTC_000015992–000016005

Folder label: “525 X 5/10/02 A 5/13/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\051302\LBB0513.D Vial: 12 ' Acq On : 13 May 2002 8:50 pm Operator: Bohlk / Inst 213 Sample : LB 5/13/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 14 10:00:21 2002 Quant Results File: 050802.RES

Quant Method : C:\MSDCHEM\l\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue May 14 09:56:07 2002 Response via : Initial Calibration DataAcq Meth : 050802

Internal Standards R.Ti Qlon Response Cone Units Dev(Min)

1) Acenaphthene-diO 18.21 164 1060019 5.00 ug/L 0.00 9) Phenanthrene d-10 22.53 188 1659057 5.00 ug/L 0.00 19) Chrysene d-12 30.32 240 1044771 5.00 ug/L 0.00 25) p-Terphenyl d-14 27.42 244 1184305 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 314159 4.98 ug/L 0.00 Spiked Amount 5.000 Recovery = 99.60% 20) Triphenyl Phosphate 29.60 326 241242 4.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.60% 21) Perylene D-12 34.33 264 526497 3.52 ug/L 0.00 Spiked Amount 5.000 Recovery = 70.40% 26) Acenaphthene d-10 (surr) 18.21 164 1060019 3.58 ug/L 0.00 Spiked Amount 5.000 Recovery = 71.60% 27) Phenanthrene d-10 (surr) 22.53 188 1659057 3.92 ug/L 0.00 Spiked Amount 5.000 Recovery = 78.40% 28) Chrysene d-12 (surr) 30.32 240 1044771 3.88 ug/L 0.00 Spiked Amount 5.000 Recovery = 77.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dini totoluene 0.00 165 0 N.D. 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. 23) Bis (2-Ethylhexyl) phthala 30.98 149 20870 0.09 ug/L 91 24) Benzo (a) pyrene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration LBB0513.D 050802.M Tue May 14 10:01:39 2002 Page 1

NYC-WTC_000015992

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NYC-WTC_000015992Source: NYC Law Department, mirrored locally

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GCMS blank results, April 2002 · Box DEP Box 57

NYC-WTC_000060990

Gas chromatography mass spectrometry blank analysis report showing non-detect levels for various organic compounds.

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