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← Document results/DEP Box 15/525 X 5/10/02 A 5/13/02
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Laboratory blank analysis results, sample AE11755, May 2002

Machine-extracted title · confidence 90%

Blank analysis for sample AE11755 to verify absence of contamination in laboratory equipment and procedures, completed May 13, 2002.

NYC-WTC_000016024–000016054

Folder label: “525 X 5/10/02 A 5/13/02

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Scanned page image, NYC-WTC_000016025
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\051302\LBA0513.D Vial: 8 ’ Acq On : 13 May 2002 5:46 pm Operator: Bohlk / Inst 213 Sample : LB 5/10/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 14 09:57:46 2002 Quant Results File: 050802.RES

Quant Method : C:\MSDCHEM\l\5973N\050802.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Tue May 14 09:56:07 2002 Response via : Initial Calibration DataAcq Meth : 050802

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 18.21 164 1036613 5.00 ug/L 0.00 9) Phenanthrene d-10 22.53 188 1576391 5.00 ug/L 0.00 19) Chrysene d-12 30.32 240 954345 5.00 ug/L 0.00 25) p-Terphenyl d-14 27.42 244 986685 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 312274 5.07 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.40% 20) Triphenyl Phosphate 29.60 326 220070 4.68 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.60% 21) Perylene D-12. 34.33 264 472344 3.46 ug/L 0.00 Spiked Amount 5.000 Recovery = 69.20% 26) Acenaphthene d-10 (surr) 18.21 164 1036613 4.21 ug/L 0.00 Spiked Amount 5.000 Recovery = 84.20% 27) Phenanthrene d-10 (surr) 22.53 188 1576391 4.47 ug/L 0.00 Spiked Amount 5.000 Recovery = 89.40% 28) Chrysene d-12 (surr) 30.32 240 954345 4.25 ug/L 0.00 Spiked Amount 5.000 Recovery = 85.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. 23) Bis (2-Ethylhexyl) phthala 30.99 149 599920 2.91 ug/L 98 24) Benzo (a) pyrene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration LBA0513.D 050802.M Tue May 14 09:59:40 2002 Page 1

NYC-WTC_000016025

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NYC-WTC_000016025Source: NYC Law Department, mirrored locally

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