NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\1\DATA\051302\LBA0513.D Vial: 8
’ Acq On : 13 May 2002 5:46 pm Operator: Bohlk / Inst 213
Sample : LB 5/10/02 Inst : Instrumen
Mise : Multiplr: 1.00
MS Integration Params: rteint.p
Quant Time: May 14 09:57:46 2002 Quant Results File: 050802.RES
Quant Method : C:\MSDCHEM\l\5973N\050802.M (RTE Integrator)
Title : Quantitation For Method 525.2
Last Update : Tue May 14 09:56:07 2002
Response via : Initial Calibration
DataAcq Meth : 050802
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-dlO 18.21 164 1036613 5.00 ug/L 0.00
9) Phenanthrene d-10 22.53 188 1576391 5.00 ug/L 0.00
19) Chrysene d-12 30.32 240 954345 5.00 ug/L 0.00
25) p-Terphenyl d-14 27.42 244 986685 5.00 ug/L 0.00
System Monitoring Compounds
2) 1,3-Dimethyl-2-nitrobenzen 13.13 134 312274 5.07 ug/L 0.00
Spiked Amount 5.000 Recovery = 101.40%
20) Triphenyl Phosphate 29.60 326 220070 4.68 ug/L 0.00
Spiked Amount 5.000 Recovery = 93.60%
21) Perylene D-12. 34.33 264 472344 3.46 ug/L 0.00
Spiked Amount 5.000 Recovery = 69.20%
26) Acenaphthene d-10 (surr) 18.21 164 1036613 4.21 ug/L 0.00
Spiked Amount 5.000 Recovery = 84.20%
27) Phenanthrene d-10 (surr) 22.53 188 1576391 4.47 ug/L 0.00
Spiked Amount 5.000 Recovery = 89.40%
28) Chrysene d-12 (surr) 30.32 240 954345 4.25 ug/L 0.00
Spiked Amount 5.000 Recovery = 85.00%
Target Compounds Qvalue
3) Hexachlorocyclopentadiene 0.00 237 0 N.D.
4) Hexachlorobenzene 0.00 284 0 N.D.
5) EPTC 0.00 128 0 N.D.
6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d
7) 2,4-Dinitotoluene 0.00 165 0 N.D.
8) Molinate 0.00 126 0 N.D.
10) Simazine 0.00 201 0 N.D.
11) Atrazine 0.00 200 0 N.D.
12) Alachlor 0.00 160 0 N.D.
13) Terbacil 0.00 117 0 N.D.
14) Acetochlor 0.00 146 0 N.D.
15) Metribuzin 0.00 198 0 N.D.
16) Metolachlor 0.00 162 0 N.D.
17) Butachlor 0.00 160 0 N.D. d
18) 4,4'-DDE 0.00 246 0 N.D.
22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D.
23) Bis (2-Ethylhexyl) phthala 30.99 149 599920 2.91 ug/L 98
24) Benzo (a) pyrene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration
LBA0513.D 050802.M Tue May 14 09:59:40 2002 Page 1
NYC-WTC_000016025
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