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Sample AE10187 analysis results, May 2002

Machine-extracted title · confidence 90%

Analytical results for sample AE10187 analyzed on May 6, 2002, listing compounds detected below the method detection limit.

NYC-WTC_000082581–000082617

Folder label: “525 X 4/30/02 A 5/1/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\050202\10187 .D Vial: 23 Acq On 2 May 2002 7:46 pm Operator: Bohlk / Inst 213 Sample SAMPLE 10187 4/30/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 06 15:02:31 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon May 06 12:42:26 2002 Response via : Initial Calibration DataAcq Meth : 050102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 17.59 164 2887198 5.00 ug/L 0.00 9) Phenanthrene d-lO 21.89 188 4561612 5.00 ug/L 0.00 19) Chrysene d-12 29.62 240 3035920 5.00 ug/L 0.00 25) p-Terphenyl d-14 26.77 244 3516352m 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.55 134 770338 5.84 ug/L 0.00 Spiked Amount 5.000 Recovery = 116.80% 20) Triphenyl Phosphate 2 8.94 326 842496 6.23 ug/L 0.00 21) Perylene D-12 33.60 264 355754 0.84 ug/L 0.00 Spiked Amount 5.000 Recovery = 16.80% 26) Acenaphthene d-10 (surr) 17.59 164 2887198 3.30 ug/L 0.00 Spiked Amount 5.000 Recovery = 66.00% 27) Phenanthrene d-10 (surr) 21.89 188 4561612 3.82 ug/L 0.00 Spiked Amount 5.000 Recovery = 76.40% 28) Chrysene d-12. (surr) 29.62 240 3035920 3.83 ug/L 0.00 Spiked Amount 5.000 Recovery = 76.60%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. . 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4’-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 0.00 129 0 N.D. d 23) Bis (2-Ethylhexyl) phthala 30.31 149 195093 1.54 ug/L 89 24) Benzo (a) pyrene 33.47 252 22029m 0.80 ug/L

(#) = qualifier out of range (m) = manual integration 10187.D 050102.M Mon May 06 17:53:17 2002 Page 1

NYC-WTC_000082585

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NYC-WTC_000082585Source: NYC Law Department, mirrored locally

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