Calibration standard analysis results, sample C5, May 2002

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Results for calibration standards including deuterated compounds analyzed on May 6, 2002.

NYC-WTC_000082506–000082517

Folder label: “525 X 4/30/02 A 5/1/02”

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Quantitation Report (QT Reviewed)

• Data File C:\MSDCHEM\l\DATA\050102\C01A0501.D Vial: 3 Acq On 1 May 2002 1:44 pm Operator: Bohlk / Inst 213 Sample CO.l Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: May 06 13:11:31 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\l\5973N\050102.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Mon May 06 12:42:26 2002 Response via : Initial Calibration DataAcq Meth : 050102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 17.59 164 3518327 5.00 ug/L 0.00 9) Phenanthrene d-10 21.89 188 4770480 5.00 ug/L 0.00 19) Chrysene d-12 29.62 240 3154217 5.00 ug/L 0.00 25) p-Terphenyl d-14 26.77 244 3046756m 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.55 134 829400 5.16 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.20% 20) Triphenyl Phosphate 28.94 326 502789 3.58 ug/L 0.00 21) Perylene D-12 33.60 264 1793525 4.09 ug/L 0.00 Spiked Amount 5.000 Recovery = 81.80% 26) Acenaphthene d-10 (surr) 17.59 164 3518327 4.64 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.80% 27) Phenanthrene d-10 (surr) 21.89 188 4770480 4.61 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.20% 28) Chrysene d-12 (surr) 29.62 240 3154217 4.59 ug/L . 0.00 Spiked Amount 5.000 Recovery = 91.80%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 20.84 284 20657m 0.09 ug/L 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene O.OO 165 0 N.D. d 8) Molinate 0.00 126 0 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. d 13) Terbacil 0.00 117 0 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 24.20 162 16190 0.02 ug/L 73 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 26.66 246 10104 0.05 ug/L 90 22) Bis (2-Ethylhexyl) adipate 28.90 129 6443 1.57 ug/L 93 23) Bis (2-Ethylhexyl) phthala 30.31 149 14601m 1.33 ug/L 24) Benzo (a) pyrene 33.44 252 7723m 0.78 ug/L

(#) = qualifier out of range (m) = manual integration C01A0501.D 050102.M Mon May 06 13:14:40 2002 Page 1

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Method 525.2 compound analysis results, May 2002 · Box DEP Box 65

NYC-WTC_000082495

Analytical results for organic compounds including hexachlorobenzene and EPTC using Method 525.2 in early May 2002.

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