Quality control data for a calibration verification sample analysis of PAHs with recovery rates between 103 and 110 percent.
NYC-WTC_000058157–000058158Folder label: “525 X 1/11/02 A 1/26/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\MSDCHEM\l\DATA\012502A\C5.D Vial: 18 Acg On : 2 6 Jan 2 002 3:25 am Operator: McLean Sample : CCV Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.p Quant Time: Jan 28 12:29:03 2002 Quant Results File: 012402B.RES
Quant Method : C:\MSDCHEM\1\5973N\012402B.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Fri Jan 25 11:19:14 2002 Response via : Initial Calibration DataAcq Meth : 012402DF
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) Acenaphthene-diO 17.96 164 15444374 5.00 ug/L 0.00 9) Phenanthrene D-10 22.27 188 19217274 5.00 ug/L 0.00 20) Chrysene D-12 30.03 240 14715878 5.00 ug/L 0.00
System Monitoring Compounds 2) 1,3-Dimethyl-2-nitrobenzen 12.89 134 4086881 5.16 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.20% 19) Triphenyl Phosphate 29.33 326 3191600 5.51 ug/L 0.00 Spiked Amount 5.000 Recovery = 110.20% 21) Perylene D-12 34.02 264 9993411 4.78 ug/L 0.00 Spiked Amount 5.000 Recovery = 95.60%
Target Compounds Qvalue 3) Hexachlorocyclopentadiene 15.47 237 752607 2.26 ug/L 98 4) Hexachlorobenzene 21.14 284 1879692 2.07 ug/L 97 5) EPTC 15.95 128 2870877 2.07 ug/L 100 0 6) 2,6-Dinitrotoluene 17.53 165 982687 2.09 ug/L 97 7) 2,4-Dinitotoluene 18.68 165 1035581 2.04 ug/L 95 8) Molinate 18.85 126 4189341 2.17 ug/L 91 10) Simazine 21.69 201 1066041 2.24 ug/L 98 11) Atrazine 21.81 200 1682547 2.15 ug/L 99 12) Alachlor 23.67 160 1591438 2.11 ug/L 95 13) Terbacil 22.61 161 1548132 2.63 ug/L 99 14) Acetochlor 23.46 146 1054361 2.18 ug/L 89 15) Metribuzin 23.48 198 1728321 2.32 ug/L 98 16) Metolachlor 24.58 162 4786341 2.17 ug/L 96 17) Butachlor 26.41 160 1403752 2.13 ug/L 83 18) 4,4'-DDE 27.04 246 1602009 2.10 ug/L 96 22) Bis (2-Ethylhexyl) adipate 29.27 129 3192901 2.19 ug/L 98 23) Bis (2-Ethylhexyl) phthala 30.70 149 5193703 2.13 ug/L 99 24) Benzo (a) pyrene 33.87 252 5083851 1.98 ug/L 98
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(#) = qualifier out of range (m) = manual integration C5.D 012402B.M Mon Jan 28 12:29:37 2002 Page 1
NYC-WTC_000058157
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NYC-WTC_000058153
Laboratory report listing analytical results for PAHs and surrogates with recovery rates on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.982
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055375
Quality control lab blank results for Method 525.2 showing detection limits for various pesticides and contaminants.
1 shared topics · Same agency, volume and box · similarity 0.973
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058155
Instrument log showing retention times and recovery percentages for PAHs in a reference standard on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.971
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055380
Calibration standard results for Method 525.2 listing concentrations and detection limits for target compounds.
1 shared topics · Same agency, volume and box · similarity 0.971
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055439
Laboratory results for sample AD28046 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.968
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055421
Laboratory results for sample AD27986 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.968
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055445
Laboratory results for sample AD28047 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.967
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055481
Laboratory results for sample AD28167 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.967
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055475
Laboratory results for sample AD28166 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.966
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055385
Reference standard results for Method 525.2 verifying analytical performance for pesticides and organic compounds.
1 shared topics · Same agency, volume and box · similarity 0.966
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000055463
Laboratory results for sample AD28106 analyzing pesticides and organic contaminants using Method 525.2.
1 shared topics · Same agency, volume and box · similarity 0.966
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000082506
Results for calibration standards including deuterated compounds analyzed on May 6, 2002.
1 shared topics · similarity 0.970
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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Fragmented document header containing identification codes and date ranges from the January 2002 collection.
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Lab analysis of sample AD28043 for pesticide and chemical residues, all results below method detection limits, completed Jan 29, 2002.
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NYC-WTC_000058153
Laboratory report listing analytical results for PAHs and surrogates with recovery rates on January 28, 2002.
Filed in the same folder
NYC-WTC_000058155
Instrument log showing retention times and recovery percentages for PAHs in a reference standard on January 28, 2002.
Filed in the same folder